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December 19, 1986 Harding Lawson Associates <br /> 4167,154.02 <br /> Exxon Company, U.S.A. <br /> Mr. Kent Sanderson <br /> Page 3 <br /> used the data to evaluate the vertical extent of hydrocarbons. Soils <br /> were removed to an approximate total depth of 20 to 21 feet below grade, <br /> which was the maximum capability of the backhoe equipment provided by <br /> AEMC. Ground water was observed in the excavation at this depth. Seven <br /> soil samples (EX-1 through EX-7) and one ground-water sample (GW-1) were <br /> collected on September 23, 1986 from the deepened excavation floor. <br /> Soil was brought to the surface by means of a backhoe bucket and sampled <br /> using an Alconox-cleaned stainless steel tube. After the cuter 3 inches <br /> of exposed soil had been removed, the sample tube was filled completely, <br /> capped with aluminum foil and a plastic slip cap at each end, sealed with <br /> tape, labeled, and stored on ice until delivery under chain of custody to <br /> a state-certified laboratory. Each of the seven soil samples were ana- <br /> lyzed for total petroleum hydrocarbons (TPH) using a gasoline standard to <br /> a detection limit of 10 parts per million (prm) and for benzene, toluene, <br /> and xylene (BTX) to a detection limit of 0.05 ppm by EPA Method 602. All <br /> samples were analyzed by Analytical Science Associates (ASA) of <br /> Emeryville, California. <br /> Ground-water sample GW-1 was collected <br /> stainless steel bailer and was decanted from within the excavation using ainto two laboratory-prepared <br /> volatile organic analysis vials, filled completely to eliminate any void <br /> space, capped with a Teflon-lined cap, labeled, and stored on ice until <br /> delivery to ASA the same day. Sample GW-1 was analyzed for TM using a <br /> gasoline standard to a detection limit of 50 parts per billion (ppb) and <br /> for BTX. to a detection limit of 1 ppb using EpA Method 602. <br /> Ms. Laurie Cottulla of the S7CLHD was present ming the roil excavation <br /> and sampling. <br /> Soil Aeration and Sampling procedures <br /> A total of 300 cubic yards of excavated soils were aerated on site between <br /> September 9, and November 21, 1986 in accordance with the requirements of <br /> the S7CAPD. Prior to aeration, stockpiled soils were vapor-surveyed <br /> using an OVA at a minimum, of 12 locations per 50 cubic yards of soil. <br /> Vapor survey locations were recorded on a field map and vapor readings <br /> were tabulated. Soil samples were collected from 18 inches below the <br /> exposed stockpile surface at the four "worst casept locations for each 50 <br /> cubic yards and were comoosited. The six composited samples were ana- <br /> lyzed by ASA for TPH using a gasoline standard. An Alccnox-cleaned <br /> stainless steel tube was advanced into the soil and comp cted until <br /> c letely filled, carcec3 with altsninum foil and plastic slip caps, <br /> sealed with tape, labeled, and stored cn ioe until delivery under cl^ain <br /> of custody to ASA. <br />