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Sequoia 680 Chesapeake Drive Redwood City CA 94063 (415) 364 9600 FAX(415) 364 9233 <br /> 4 404 N Wiget Lane Walnut Creek CA 94598 (510) 988 9600 FAX(510) 988 9673 <br /> DD- Analytical 819 Striker Avenue,Suite 8 Sacramento CA 95834 (916) 921 9600 FAX(916)921 0100 <br /> Blaine Technical Services Client Prot ID Shell, Stockton, 960820-K1 Sampled 08/20/96 <br /> 985 Timothy Drive Sample Descript MW4 Received 08/22/96 <br /> San Jose, CA 95133 Matrix LIQUID <br />_ Analysis Method EPA 8260 Analyzed 09/04/96 <br /> Attention Fran Thie Lab Number 9608E66-04 _ Reported 09JO9196 <br /> QC Batch Number MS0903968260F3A <br /> Instrument ID F3 <br /> Methyl t-Butyl Ether (MTBE) <br /> Analyte Detection Limit Sample Results <br /> ug/L. ug/L <br /> Methyl t-Butyl Ether - 20 32 <br /> Surrogates Control Limits % % Recovery <br /> 1,2-Dichloroethane-d4 76 114 114 <br /> Toluene-d8 88 110 99 <br /> 4-Bromofluorobenzene 86 115 101 <br /> Analytes reporte s N D were not present above the stated limit of detection <br /> SE I A ALYTICAL - ELAP #1210 <br /> Penner <br /> ec <br /> ect Manager Page 4 <br />