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Sequoia 680 Chesapeake Drive Redwood City CA 94063 (415) 364 9600 FAX(415) 364 9233 <br /> 4 4 404 N Wiget Lane Walnut Creek,CA 94598 (510) 988 9600 FAX(510)988 9673 <br /> X11 — Analytical 819 Striker Avenue Suite 8 Sacramento CA 95834 (916) 921 9600 FAX(916)921 0100 <br /> Blaine Technical Services Client Prod ID Shell Stockton/961125-A3 Sampled 11/25/96 <br /> 985 Timothy Drive Sample Descript MW-4 Received 11/27/96 <br /> San Jose, CA 95133 Matrix LIQUID <br /> Analysis Method 8015Mod/8020 Analyzed 12/05/96 <br /> Attention Fran Thie Lab Number 9611122-04 Reported 12111/96 <br /> QC Batch Number GC120596BTEX21A <br /> Instrument ID GCHP21 <br /> Total Purgeable Petroleum Hydrocarbons (TPPH) with BTEX and MTBE <br /> Analyte Detection Limit Sample Results <br /> ug/L ug/L. <br /> TPPH as Gas 50 N D <br /> Methyl t-Butyl Ether 25 21 <br /> Benzene 0 50 N D <br /> Toluene 050 N D <br /> Ethyl Benzene 0 50 N D <br /> Xylenes (Total) 0 50 0 98 <br /> Chromatogram Pattern <br /> Surrogates Control Limits% % Recovery <br /> Trifluorotoluene 70 130 96 <br /> Analytes reported as N D were not present above the stated limit of detection <br /> S A NALYTICAL - ELAP #1210 <br /> 1-11 <br /> Penner <br /> Oect Manager Page 4 <br />