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--__ _— _— ------ r IV W-JI r— I I Z iJ <br />' 4D Sequoia 4455 McDowell SM*rM.Ste D <br /> i Petaluma.CA W54 <br /> qQF Analytical (707) 792-I845 <br /> FAX{7071 742-0342 <br /> Project: Unocal/Tosco Sampled 5/18/99 <br /> Digital Dr Sulre 100 Project Number 5098 STO Unzon/227903UN4 Received 5124199 <br /> NOVOW,CA 94949 Pra eat M (31etm M3ttuecci <br /> Reported. 618/99 <br /> Ta l PetxpleIn$174 WCrh0lla Alit GS001ti10 0n11 BT ''''fir by)VA 801"020vot wity CoUtMI <br /> S0gb4»E AjpOlyflM-jPoWtim <br /> Analyte Date spike Stlrnple QC Reporting limit R000v "D RPD <br /> Anel level Result Result Units Recov !amts °/a [rout <br /> 1pk 90509]1 to E 0/99 & etbod- EP 5030 sats <br /> S�Ank 050911- K! <br /> 1Ilne 5130199 ND Msft 0.400 <br /> enzenc ND " 0.00200 <br /> Toluene " ND " 000200 <br /> ylbenzene " <br /> ND 0A0200 <br /> ylenes total) to ND " 0.00400 <br /> urmgate a,a,a-Y}efluorwbftw re " 0 300 0 285 " 650-135 950 <br /> S'urrogate 4-BrantufTporabett2ene " 0 300 0 269 650-135 897 <br /> CS 4050911-$S2 <br /> Gasoline _ 5/30/99 2,00 197 650-135 985 _ <br /> unnsgte 4-BromaJluoraberraene of0 300 0 267 " 650-135 890 <br /> C 245,0931-BS3 <br /> Ben 5130199 0200 0 181 m9/kg 650-139 905 <br /> uene 0200 0179 " 650-135 895 <br /> ylbenzcne a 0.200 0 179 65O-I35 89 5 <br /> 6enes <br /> (otw) " 0 600 0 538 " 65,0-135 99 7 <br /> Surrogate q,a,a-9}rftuoratoluene " 01300 0178 ° 6S 0-135 91 7 -- <br /> LAtrix Sol 050911.. P90368_6x02 <br /> Gasoline 5/30199 2 00 ND l 87 MWJ,g 650-135 93.5 <br /> S ik( ogate' Q-BromoJluorobenzene " 0 300 0 234 " 650-135 780 <br /> MIgirrixe. ! - 9050911-MS2 2905656-02 <br /> Benzene 5/30199 0200 ND 0 199 nisft 650-135 99 S <br /> oluene " 0200 ND 0 192 650-135 96 0 <br /> thyllsonzene " 0.200 ND 0 189 " 650-13S 94.5 <br /> Xylenes(total) 0 600 ND 0 569 " 650-135 94.8 <br /> rrogate a,a,a-7h49(u rotoluena " 0,300 0301 " - — <br /> 65 D-133 100 <br /> atnx S 1 u Q050911-MSD1 2MLkS642 <br /> Gasoline 5/30/99 2 00 ND 197 65 06135 98.5 200 5.21 _ <br /> rrogate 4 Bramoflaoroberw4w if0 300 0 238 " 650-135 793 <br /> t&tV!r-5vjke <br /> Duo 905091I-MBD2 0905 <br /> Benzene 5/30199 0200 ND 0 197 <br /> toluene 0 2� 650-135 98.5 20 0 1.01ylbenzone ,� ND 0 190 " 65,0.135 95.0 200 105 <br /> 0100 ND 0 187 " 650-135 93 5 20 0 1.66 <br /> Xylenes(total) _ 0.600 ND 0 562 ^ <br /> 650-135 937 200 1.17 <br /> rrogate a,Al.a-Trf luoratoluene " 0 300 0.300 " 650-135 100 <br /> uola Anal al-Petaluma <br /> 9 Analyticiii to Brsd of naporl forte#of mores and donloons <br /> Page 3 oF5 <br />