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CALIFORNIA LABORATORY SERVICES ' <br /> e <br /> 09/29/04 13 30 ' <br /> ENSR-Sacramento Project Former Unocal 5098,5606 09 �v Sto kta <br /> 10411 Old Placerville Rd,Suite 210 Project Number 06940-293-100 C �'1'or4C Order 'CiVIU746 <br /> Sacramento,CA 95827-2508 Project Manager Ben I Ilenmgburg COC# 41080 <br /> Polynuclear Aromatic Compounds by EPA Method 8310 - Quality Control ' <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %MEC Limits RPD Limit Notes <br /> Batch CN07384-FPA 3510B HPLC <br /> Blank(CN07384-BLK1) Prepared 09/23/04 Analyzed 09/27/04 <br /> Acenaphthene ND 020 µg/L <br /> Acenaphthylene ND 020 " <br /> Anthracene ND 020 <br /> Benzo(a)anthracene ND 020 " <br /> Benzo(a)pyrene ND 020 " <br /> Benzo(b)fluoranthene ND 020 " <br /> Benzo(g h i)perylene ND- 020 <br /> Benzo(k)fluoranthene ND 020 " <br /> Chrysene ND 020 " <br /> Dibenz(ah)anthracene - ND 020 <br /> Fluoranthene ND 020 " <br /> Fluorene ND 020 " <br /> Indeno(1,2,3-cd)pyrene ND 020 " <br /> Naphthalene ND 020 <br /> Phenanthrene ND 020 " <br /> Pyrene ND 020- <br /> Surrogate <br /> 20 "Surrogate Terphenyl-&4 0 796 100 796 70-130 - <br /> LCS(CN07384-BSI) Prepared 09/23/04 Analyzed 09/27/04 <br /> - --Benzo(g,h,i)perylene - -- -- - - - =0 994-- 0 20 µg/L- --] 00--- - =-99 4 -50-116 -- ---- - - - - -- <br /> Chrysene 1 11 020 1 00 HI 50-190 <br /> Phenanthrene 119 020 100 119 50-155 <br /> ` Surrogate Terphenyl-d14- - -' 0 804 -- 100 ` -804 70-130 - <br /> LCS Dup(CN07384-ESDI) Prepared 09/23/04 Analyzed 09/27/04 ' <br /> Benzo(g h 4 perylene 102 _ 020 µg/L too 102 50-116 258 35 <br /> Chrysene 1 14 020 1 00 114 50-190 267 35 <br /> Phenanthrene 1 20 020 1 00 120 50-155 0 837 35 <br /> Surrogate Terphenyl-d14 0 818 100 818 70-130 ' <br /> CA DOHS ELAP Accreditation/Registration Number 1233 1 <br /> 3249 Fitzgerald Road Rancho Cordova, CA 95742 www californlalab com 916-638-7301 Fax: 916-638-4510 <br />