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+ . 819 Sinker Ave Ste 8 <br /> S e q u o 1►a Sacramento CA 95834 <br /> (916)921-9600 <br /> Analytical PAX(916)921-0104 <br /> www sequoiaiabs wm <br /> G tiler-Ryan-Dublin Project Former Unocal 5098, Stockton,CA S302592 <br /> Sierra Court, Ste J Project Number N/A Reported <br /> m CA,94568 Project Manager Deanna L Harding 03/10/03 17 17 <br /> Total Purgeable Hydrocarbons by DHS LUFT- Quality Control <br /> Sequoia Analytical - Sacramento <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RFD Limit Notes <br /> itch 3030007-EPA 5030B(P/T) ....._,... -•--,-.—,,._..., <br /> Matrix Spike Dup(3030007-MSDI) Source 5302592-05 Prepared&Analyzed 03/03/03 <br /> rgeable Hydrocarbons 264 50 ug/I 250 ND 114 60-140 1 25 <br /> Suri ogate a a a-T)tfluorotaluene 982 lO 0 98 60-140 <br /> latch 3030032-EPA 5030E(P/T <br /> Blank(3030032-BLKI) Prepared& Analyzed 03/03/03 <br /> rgeable Hydrocarbons ND 50 ug/1 <br /> Surrogate a a a-Tv ifluorotoluene 849 100 85 60-140 <br /> lank(3030032-BLK2) Prepared&Analyzed 03/04/03 <br /> Purgeable Hydrocarbons ND 50 ug/I <br /> WwrOugate a a a Trifluorotoluene 891 100 89 60 140 <br /> Blank(3030032-BLK3) Prepared&Analyzed 03/05/03 <br /> rgeable Hydrocarbons ND 50 ug/l <br /> ti rugate a a a Tii/luoiotoluene 857 100 86 60 140 <br /> Laboratory Control Sample(3030032-BSI) Prepared& Analyzed 03/03/03 <br /> rgeable Hydrocarbons 271 50 ug/l 250 108 70 130 <br /> Sun ogate a a a Trifluot otoluene 9 74 100 97 60-140 <br /> laboratory Control Sample(3030032-BS2) Prepared& Analyzed 03/04/03 <br /> Purgeable Hydrocarbons 267 50 ug/i 250 107 70 130 <br /> i rogaie a a a Tri luoiotoluene 102 100 107 60 140 - <br /> Itaboratory Control Sample(3030032-BS3) _ Prepared& Analyzed 03/05/03 <br /> Vurgeable Hydrocarbons 258 50 ug/I _.... .. 250 . .. 103 70-130 <br /> ota Analytical - Sacramento The i esults in this t epos t apply to the samples analyzed to accordance with the chain of <br /> custody document Unless otherwise stared, results are t eported on a wet weight basis <br /> This analytical i eport must be reproduced in its entirety <br /> Page 97 of 126 <br />