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8 19 <br /> ker <br /> Sequoia Sacramento, <br /> 4 <br /> Sacramerno,CA 95834 <br /> Analytical (916)921-0100 <br /> FAX(916)921-0140 <br /> www sequoislabs cam <br /> Gettler-Ryan-Dublin Project Former Unocal 5098,Stockton,CA 5302592 <br /> 6747 Sierra Court,Ste J Project Number NIA Reported <br /> Dublin CA,94568 Prosect Manager Deanna L Harding 03/10/03 17 17 <br /> Volatile Organic Compounds by EPA Method 8260B - Quality Control <br /> Sequoia Analytical - Sacramento l T_ <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch 3020415-EPA 5030B IP/T] <br /> Matrix Spike Dup(3020415-MSDI) Source S302592-23 Prepared&Analyzed 02/28/03 <br /> Sun ogare Toluene-dB 275 249/1 250 110 70-130 <br /> Suri ogare 4-BFB 276 250 110 70-130 <br /> Batch 3030025- EPA 5030B IP/TJ <br /> Blank(3030025-BL,KI) Prepared&Analyzed 03/04/03 <br /> Benzene ND 050 ugA <br /> Bromobenzene ND 050 " <br /> 'pen-bury]alcohol ND 100 w <br /> Bromochloromethane ND 050 " <br /> 13romodichloromethane ND 050 <br /> Di-isopropyl ether ND 20 " <br /> Bromoform _ ND 050 " <br /> Ethyl ten-butyl ether ND 20 <br /> Bromomethane ND 10 " <br /> Tert-amyl methyl ether ND 20 " <br /> Ethanol ND 500 <br /> n Butylbenzene ND 050 <br /> 1;2-Dichloroethane ND 20 " <br /> sec-Butylbenzene ND 050 <br /> 1,2-Dtb�r-omoethana(EDB) --T -ND 2 0 { <br /> tert-Butylbenzene ND 050 " <br /> Carbon tetrachloride T ND 050 " <br /> Cblorobenzene — l` -. __ ND _ 050 <br /> _- <br /> Chloroethane- - -ND <br /> Chloroform ND G50 " <br /> Chloromethane ND 10 <br /> 2-Chlorotoluene - ND 050 - <br /> 4-Chlorotoluene ND 050 " <br /> Dibromochloromethane ND 050 <br /> 1,2-Dibromoethane(EDB) ND 050 " <br /> Dibromomethane. ND 050 " <br /> 1,2-Dibromo 3-chloropropane ND 10 <br /> 1,2-Dichlorobenzene - ND 050 " <br /> 1,3-Dichlorobenzene ND - __ _ 050 <br /> 1,4-Dichlorobenzene ND 050 <br /> Sequoia Analytical - Sacramento The results in this report apply to the samples analyzed in accordance with the churn of <br /> custody document Unless otherwise stated r esults are reported on a wet weight basis <br /> This analytical report must be reproduced in its entirety <br /> Page 110 of 126 <br />