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Sequoia <br /> 819 Striker Ave Ste 8 <br /> Sacramento,CA 95834 <br /> Analytical <br /> (916)921-9600 <br /> FAX(916)921-0100 <br /> ettler-Ryan-Dublin Project Fortner Unocal 5098,Stockton,CA 5212135 <br /> 6747 Sierra Court,Ste J Project Number NIA Reported <br /> Dublm CA,94568 Project Manager Deanna L Harding 12127102 14 I4 <br /> Volatile Organic Compounds by EPA Method 8260B- Quality Control <br /> Sequoia Analytical-Sacramento <br /> Reporting Spike Source %REC RPD <br /> Lyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch 2120259-EPA 5030B[PIT] <br /> Blank(2120259-BLKII Prepared&Analyzed 12/16/02 <br /> trans-l,2-Dichloroethene ND 050 ug/l <br /> 1,2-Dichloropropane ND 050 <br /> 1,3-Dichloropropane ND 0 50 " <br /> 2,2-Dichloropropane ND 0 50 " <br /> 1,1-Dichloropropene ND 050 " <br /> Ethylbenzene ND 0 50 " <br /> Hexachlorobutadiene ND 10 <br /> Isopropylbenzene ND 0 50 " <br /> p-Isopropyltoluene ND 0 50 " <br /> Methylene chloride ND 1 0 <br /> Methyl tert-butyl ether ND 0 50 " <br /> Naphthalene ND 2 0 <br /> n-Propylbenzene ND 0 50 " <br /> W <br /> ne ND 0 50,2-Tetrachloroethane ND 0 50 " <br /> 1,1,2,2-Tetrachloroethane ND 10 " <br /> Tetrachloroethene ND 0 50 11 <br /> i <br /> Toluene ND 0 50 <br /> 1,2,3-Trichlorobenzene ND 0 50 <br /> 1,2,4-Tnchlorobenzene ND 0 50 " <br /> 1,1,1-Trichloroethane ND 0 50 " <br /> 1,1,2-Trichloroethane ND 0 50 " <br /> Trichloroethene ND 0 50 " <br /> Trichlorofluoromethane ND 0 50 <br /> 1,2,3-Trichloropropane ND 10 <br /> 1,2,4-Trimetbylbenzene ND 0 50 " <br /> 1,3,5-Trimethylbenzene ND 0 50 " <br /> Vinyl chloride ND 0 50 <br /> Xylenes(total) ND 0 50 <br /> Surrogate 12-DCA-d4 221 25 0 88 60-140 <br /> Surrogate Dioromoftuoromethane 22 4 25 0 90 70-130 <br /> Surrogate 12-DCA-d4 221 25 0 88 70-130 <br /> Surrogate Toluene-d8 278 250 111 70-130 <br /> Surrogate 4-BFB 24 7 250 99 70-130 <br /> Sequoia Analytical-Sacramento The results in this report apply to the samples analyzed in accordance with the chain <br /> of custody document Unless otherwise stated results are reported on a wet weight <br /> basis This analytical report must be reproduced in its entirety <br /> .0 <br /> 97 of 102 <br />