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r <br /> r CALIFORNIA LABORATORY SERVICES <br /> r11/05/04 15 09 <br /> ENSR-Sacramento Protect Former Unocal 5098,5606 CL W rk&OS90P CNJ0883 <br /> r10411 Old Placerville Rd,Suite 210 Project Number 06940-293-100 COC# None <br /> Sacramento,CA 95827-2508 Project Manager Ben 1 Heningburg <br />' Volatile Organic Compounds by EPA Method 8260B - Quality Control <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch CN08560- EPA 5030 Water MS <br /> rBlank(CN08560-BLKI) Prepared&Analyzed 11/03/04 <br /> 1,3,5-Tnmethylbenzene ND 050 µg/L <br /> Vinyl chloride ND 1 0 " <br /> Xylenes(total} ND 10 " <br /> Di-isopropyl ether ND 050 <br /> Ethyl ten-butyl ether ND 050 <br /> tert-Amyl methyl ether ND 050 " <br /> Tert-butyl alcohol ND 50 " <br /> Surrogate 12-Dichloroethane-d4 955 100 955 66-135 <br /> Surrogate Toluene-d8 961 100 961 72-125 <br /> ISOgale 4-Bromo luorobenzene 103 100 103 73-125 <br /> (CN08560-BS1) Prepared&Analyzed 11/03/04 <br /> Benzene 177 050 µg/L 200 885 60-135 <br /> Chlorobenzene 182 0 50 200 91 0 60-133 <br /> i,l-Dichloroethene 16 7 050 200 83 5 42-150 <br /> Toluene 176 0 50 200 880 60-137 <br /> Trichloroethene 154 050 200 77 0 62-140 <br /> Surrogate 1 2-Dichloroethane-d4 908 100 908 66-135 <br /> Surrogate Toluene-d8 9 78 100 978 72-125 <br /> Surrogate 4-Bromo luoroberuene 103 100 103 73-125 <br /> LCS Dup(CN08560-BSBI) Prepared&Analyzed 11/03/04 <br /> Benzene 177 050 µg/L 200 885 60-135 000 25 <br /> Chlorobenzene 18 0 050 11 200 90 0 60-133 1 10 25 <br /> 1,1-Dichloroethene 166 050 200 83 0 42-150 0 601 25 <br /> Toluene 175 0 50 200 87 5 60-137 0 570 25 <br /> Tnchloroethene 154 050 200 770 62-140 000 25 <br /> Surrogate 1 2-Dichloroethane-d4 904 100 904 66-135 <br /> Surrogate Toluene-d8 9 76 100 976 72-125 <br /> Surrogate 4-11romofluorobenzene 104 100 104 73-125 <br /> CA DOHS ELAP Accreditation/Registration Number 1233 <br /> 13249 Fitzgerald Road Rancho Cordova, CA 95742 www californialab com 916-638-7301 Fax 916-638-4510 <br />