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Work Order <br /> Da1c Alpha Analytical, Inc - QC Summary Report 00102645 <br /> 03 Nov-00 <br /> Tes!Code 5W82606 Batch ID MS4S1027A Analysis Date 1013412000 15 42 <br /> Method Blank <br /> Sample ID MBLK_00103016 Units pgJKg Run ID GCIMSD_4_001027 Prep Date 10!3012000 <br /> alyte Result PQL SpkVal SpkRefVal %REC LowLtmit HlghLtmrt RPD Ref Val %RPD Qual <br /> Pl=thyl tert-butyl ether(MTBE) ND 5 <br /> enzene ND 5 <br />' Toluene ND 5 <br /> Ethylbenzene ND 5 <br /> m,p-Xylene NO 5 <br /> o-Xylene NO 5 <br />' Laboratory Control Spike Test Code SW8260B Batch ID MS4S1027A Analysis Date 10127/2000 21 12 <br /> Sample ID LCS MS4S1027A Units pg/Kg Run ID GCIMSD 4_001027 Prep Date 10/2712000 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit Hight-imit RPD Ref Val %RPD Qual <br />' Methyl tent-butyl ether(MTBE) 276 5 200 138 70 142 <br /> Benzene 190 5 200 95 66 142 <br /> Toluene 205 5 200 102 59 139 <br /> Ethytbenzene 214 5 200 107 70 134 <br /> m p-Xylene 428 5 400 107 60 146 <br />' o-Xytene 212 5 200 106 52 148 <br /> Sample Matrix Spike Test Code SW82608 Batch ID MS4S1027A Analysis Date 10127/2000 21 53 <br /> Sample ID 00102645-01AMS Units pg1Kg Run lD GCIMSD 4 001027 Prep Date 1012712000 <br />' Anal Result PQL SpkVal SpkRefVal %REC Lowt-imit HighLlmit RPD Ref Val %RPD Qual <br /> Methyl tert-butyl ether(MTBE) 568 10 400 0 142 70 142 <br /> Benzene 392 10 400 0 98 66 142 <br /> Toluene 407 10 400 0 102 59 139 <br />' Ethytbenzene 429 10 400 0 107 70 134 <br /> m,p-Xylene 876 10 800 0 109 60 146 <br /> o-Xylene 435 10 400 0 109 52 148 <br />' Sample Matrix Spike Duplicate Test Code SW8260B Batch ID MS4S1027A Analysts Date 10/2712000 22 14 <br /> Sample ID 00102645-01AMSD Units pglKg Run ID GCIMSD_a 001027 Prep Date 10/27/2000 <br /> Result PQL SpkVal SpkRefVal%REC LowLlmit HighUmlt RPD Ref Val %RPD Qua] <br /> thyt tent-butyl ether(MTBE) 569 10 400 0 142 70 142 5679 0 185 <br /> Benzene 406 10 400 0 101 66 142 391 8 3 53 <br /> Toluene 420 10 400 0 105 59 139 4072 428 9 30296 <br /> Ethytbenzene 443 10 400 0 111 70 i 34 <br />' m.p-Xylene 906 10 800 0 113 60 146 875 6 3 41 <br /> o-Xylene 455 10 400 0 114 52 148 4347 451 <br /> Comments ND-Not Detected at the Reporting Limit D-it the spiked value is<25%of the reference value recovery should not be calculated <br />' S-Spike Recovery outside accepted recovery limits M-Spike Recovery outside accepted recovery limits due to matrt <br /> li-Analyte detected in the associated Method Blank <br />