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Work Order <br /> Date Alpha Analytical, Inc - QC Summary Report 00102645 <br />' 03-Nov-00 <br /> Method Blank Test Code SW8260B Batch ID MS4W1030A Analysis Date 10131/2000 01 36 <br /> Sample ID MBLK_00103044 Units }ig1L Run ID GC/MSD-4-001030 Prep Date 10/31/2000 <br /> alyte Result PQL SpkVal SpkRefVal %REC LowLimd Highl_imit RPD Ref Val %RPD Qual <br /> thyl tert-butyl ether{MTBE} ND 05 <br /> enzene NO 0 5 <br />' Toluene NO 0 5 <br /> Ethylbenzene NO 0 5 <br /> m,p-Xylene NO 0 5 <br /> o-Xylene ND 0 5 <br />' Laboratory Control Spike Test Code SW8260B Batch ID MS4W1030A Analysis Date 10/3112000 05 41 <br /> Sample ID LCS MS4Wi030A Units pglL Run ID GCIMSD_4_001030 Prep Date 10131/2000 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-tmit Hight-imit RPD Ref Val %RPD Qual <br />' Methyl tert-butyl ether(MTBE) 8 64 0 5 10 86 70 142 <br /> Benzene 101 0 5 10 101 76 127 <br /> Toluene 9 8 0 5 10 98 76 125 <br /> Ethy[benzene 105 0 5 10 105 64 132 <br /> m,p-Xylene 222 05 20 111 70 130 <br /> o-Xylene 106 0 5 10 106 70 130 <br /> Sample Matrix Spike Test Code SW8260B Batch ID MS4W1030A Analysts Date 10/3112000 06 22 <br /> Sample ID 0010260140AMS Units pg1L Run ID GCIMSD_4 001030 Prep Date 10/3112000 <br />' Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HtghUmit RPD Ref Val %RPD Qua] <br /> Methyl tert-butyl ether(MTBE) 41 2 5 50 0 82 70 142 <br /> Benzene 482 2 5 50 0 96 76 127 <br /> Toluene 472 25 50 0 94 76 125 <br />' Ethylbenzene 505 2 5 50 0 101 64 132 <br /> m,p-Xylene 107 2 5 100 0 107 70 130 <br /> o-Xylene 529 2 5 50 0 106 70 130 <br /> Sample Matrix Spike Duplicate Test Code SW82608 Batch ID MS4W1030A Analysts Date 10/31/2000 06 42 <br /> Sample lD 00102601-10AMSD Units pglL Run ID GCIMSD_4_001030 Prep Date 10131/2000 <br /> Analyte Result PQL SpkVal SpkRefVal%REC LowLumt HighUmit RPD Ref Val %RPD Qual <br /> thyl tart-butyl ether(MTBE) 43 1 2 5 50 0 86 70 142 4097 516 <br /> mane 51 2 5 50 0 102 76 127 4815 5 65 <br /> Toluene 485 25 50 0 97 76 125 4718 276 <br /> Ethylbenzene 494 25 50 0 99 64 132 50 5 2 22 <br /> m,p-Xylene 110 25 100 0 110 70 130 1075 27 <br />' o-Xylene 528 25 50 0 106 70 130 5293 0208 <br /> 1 <br /> Comments ND-Not Detected at the Reporting Limn D-II the spiked value is<25%of the reference value recovery should not be calculated <br /> S-Spike Recovery outside accepted recovery limas M Spike Recovery outside accepted recovery limits due to matrix <br /> 18-Analyte detected in the associated Method Blank <br />