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Oct -02-2007 12:18pm From- <br />McCam2bell Analytical, Inc. <br />T-982 P.009/009 F-634 <br />1534 Willow Pass Road. Pittshurg, CA 945 65-1 70 1 <br />Wcb: www.mccurnpbdl,cpm T mail main;iZm,rnrnpbaflxcm <br />WorkOrder 0703322 <br />Spiked) Sample, 1D: 0703337.004D <br />-CS-LCSD Acceptance Criteria (%) <br />% RPE MS / MSD RPD LCSILCSD RPD <br />0 75 - 125 20 35- 115 2(1 <br />0.721 75 - 125 20 35 - 115 20 <br />0.439 75 -125 20 85- IIS 20 <br />2.31 75 • 125 20 85- 115 20 <br />0.396 75 - 125 20 85- 115 20 <br />U 75- 125 20 85 - 115 20 <br />0.852 75 - 125 20 85 - I I s 20 <br />1.25 75 - 125 20 85 - 115 20 <br />1 86 75 - 125 20 85 - 115 20 <br />0.662 75- 125 20 85 - 115 20 <br />1.31 75 • 125 20 85 • 115 2U <br />0.192 75 - 125 20 85 - 115 20 <br />1.00 75- 125 20 85 - t i 5 20 <br />0.343 75 - 125 20 85 - 115 20 <br />0 75. 125 20 85- 115 20 <br />0.695 75- 125 20 85- 115 20 <br />2.3o 75- l25 2U 85 - 115 2U <br />1.36 70 - 130 20 70- 130 20 <br />All target compounds in the Method Blank of this extraction batch were ND legs than the lttdthod R1. with the following exceptions: <br />NONE <br />BATCH 26798 SUMMARY <br />Sample ID Date Sampled Date Extracted Date Analyzed Sample ID Date Sampled Date Extracted Date Analyzed <br />0703322-OOIA 03/09/07 03/14/07 03/16/07 3:46 PM 0703322-OOIA 03/09/til 03/14/07 03/19/07 5:30 PM <br />0703323-OOIA 03/09/07 03/14/07 03 <br />MS = Matrix SPikc; MSD - Matrix Spike ouptiwatc; LCS = 431Poratory Controi Sample; t.CSD = Laboratory ConVel Sample Duplicate: upGcate; RPD =Relative Percent -De, viation. <br />°6 Recovery e 100 • (MS -Sample) / (Amount Spikod); RPD = 100 ' (MS - MSD) / ((MS + MSD) 12). <br />M5 / MSD spike rtcovedes and / or °kRPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons: a) the sample Is inhomogenous AND <br />eontsins significant concentrations of anslyte relative to the amount spiked, or b) the spiked sample's matrix Interferes with the spike remvery. <br />N/A = not applicable to this method <br />NR n aMlalyto concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount roe water matrix or sample dilut.-d due to high matrix w analyte r^^• -- <br />DI IS EI AP Certification NO 1644 - QA/QC Officer <br />QC SUMMARY <br />REPORT <br />FOR <br />E200.8 <br />W.O. Sample Matrix; Water <br />QC Matrix: <br />Water <br />EPA Method E200.8 <br />Extraction E200-8 <br />BatchlD: 26796 <br />Analyte <br />Sample <br />SpikedMS <br />MSD <br />MS -MSD <br />LCS <br />LCSD <br />!tg/L <br />pg/L <br />% Rec. <br />% Rec. <br />°A RPD <br />% Rec. <br />% Rec. <br />Antimony <br />2.2 <br />10 <br />104 <br />109 <br />3.27 <br />108 <br />108 <br />Arsenic <br />4.5 <br />10 <br />105 <br />105 <br />0 <br />IOU <br />99.5 <br />Larium <br />310 <br />100 <br />114 <br />120 <br />1.44 <br />98.2 <br />97.8 <br />Beryllium <br />I ND <br />10 <br />93.7 <br />92.9 <br />0.859 <br />88.1 <br />36.1 <br />Cadmium <br />ND <br />10 <br />94.2 <br />94.2 <br />0 <br />98.4 <br />98,8 <br />Chromium <br />3.2 <br />IU <br />99.3 <br />101 <br />0.633 <br />lU0 <br />IOU <br />Cobalt <br />ND10 <br />30 <br />80.7 <br />0.892 <br />95.4 <br />94.6 <br />Copper <br />36 <br />10 <br />112 <br />110 <br />0.514 <br />99.1 <br />100 <br />Lead <br />0 55 <br />10 <br />97.5 <br />97.3 <br />0.194 <br />93.9 <br />92.1 <br />Mercury <br />0.014 <br />0.50 <br />102 <br />102 <br />0 <br />97 <br />96.3 <br />Molybdenum <br />8.4 <br />10 <br />lot <br />98.8 <br />1.25 <br />93.5 <br />92 2 <br />Nickel <br />12 <br />10 <br />98.6 <br />99.4 <br />0.0915 <br />99,1 <br />99 3 <br />Selenium <br />105 <br />0.524 <br />96.2 <br />97.2 <br />$ilvCr <br />89 <br />0.482 <br />96.4 <br />96 <br />Thallium <br />=9. <br />93.9 <br />0,287 <br />91,8 <br />91.8 <br />Vanadium <br />113 <br />0.23R <br />l00 <br />101 <br />Zinc <br />89.5 <br />0.32093.4 <br />91.3 <br />%SS; <br />1106 <br />0 <br />99 <br />97 <br />WorkOrder 0703322 <br />Spiked) Sample, 1D: 0703337.004D <br />-CS-LCSD Acceptance Criteria (%) <br />% RPE MS / MSD RPD LCSILCSD RPD <br />0 75 - 125 20 35- 115 2(1 <br />0.721 75 - 125 20 35 - 115 20 <br />0.439 75 -125 20 85- IIS 20 <br />2.31 75 • 125 20 85- 115 20 <br />0.396 75 - 125 20 85- 115 20 <br />U 75- 125 20 85 - 115 20 <br />0.852 75 - 125 20 85 - I I s 20 <br />1.25 75 - 125 20 85 - 115 20 <br />1 86 75 - 125 20 85 - 115 20 <br />0.662 75- 125 20 85 - 115 20 <br />1.31 75 • 125 20 85 • 115 2U <br />0.192 75 - 125 20 85 - 115 20 <br />1.00 75- 125 20 85 - t i 5 20 <br />0.343 75 - 125 20 85 - 115 20 <br />0 75. 125 20 85- 115 20 <br />0.695 75- 125 20 85- 115 20 <br />2.3o 75- l25 2U 85 - 115 2U <br />1.36 70 - 130 20 70- 130 20 <br />All target compounds in the Method Blank of this extraction batch were ND legs than the lttdthod R1. with the following exceptions: <br />NONE <br />BATCH 26798 SUMMARY <br />Sample ID Date Sampled Date Extracted Date Analyzed Sample ID Date Sampled Date Extracted Date Analyzed <br />0703322-OOIA 03/09/07 03/14/07 03/16/07 3:46 PM 0703322-OOIA 03/09/til 03/14/07 03/19/07 5:30 PM <br />0703323-OOIA 03/09/07 03/14/07 03 <br />MS = Matrix SPikc; MSD - Matrix Spike ouptiwatc; LCS = 431Poratory Controi Sample; t.CSD = Laboratory ConVel Sample Duplicate: upGcate; RPD =Relative Percent -De, viation. <br />°6 Recovery e 100 • (MS -Sample) / (Amount Spikod); RPD = 100 ' (MS - MSD) / ((MS + MSD) 12). <br />M5 / MSD spike rtcovedes and / or °kRPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons: a) the sample Is inhomogenous AND <br />eontsins significant concentrations of anslyte relative to the amount spiked, or b) the spiked sample's matrix Interferes with the spike remvery. <br />N/A = not applicable to this method <br />NR n aMlalyto concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount roe water matrix or sample dilut.-d due to high matrix w analyte r^^• -- <br />DI IS EI AP Certification NO 1644 - QA/QC Officer <br />