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GeoAnalytical Laboratories, Inc. <br />2300 Maryann Dr. Turlock. CA 95380 (209) 100 Fox(209)66&4516 <br />cosift tacgeo@mnd <br />Reitort # V910224 Pmjed: 25327 Jones Road, Escalon CA 95320 <br />San Joaquin County Envirownental Health <br />fm F49 maw sueet PON: PA# 197375 - <br />Stockton, CA 95202 <br />laorpule Chemistry - Quality Control <br />GeoAnatytkal Laboratorks, Inc. <br />Date: 09/14/09 <br />Dge Rwdl 09/02M <br />Reporting Spike Source 0/16REC RPD <br />A Result Limit Units LMTj Result %REC Limits RPD Limit Notes <br />fttch V00240 - 3OND <br />Source. V9*U4-0 <br />Preparvd & Analyzed: OW09M9 <br />Antimony <br />LCS Dup (VM448-BSDt) <br />0.5 mg/kg <br />5.000 <br />ND <br />66 <br />W120 QM -01 <br />Arsenic <br />5.64 <br />Ant <br />6.00 <br />0.5 <br />nqVkg 5.000 <br />120 <br />84120 <br />19 <br />20 <br />Arsenic <br />5.32 <br />0.5 <br />5.000 <br />106 <br />W120 <br />4 <br />20 <br />Barium <br />13.9 <br />0.5 <br />12.50 <br />111 <br />84120 <br />3 <br />20 <br />Beryllium <br />4.77 <br />0.5 <br />5.000 <br />95 <br />W120 <br />2 <br />20 <br />Cadmium <br />5.53 <br />0.5 <br />5.000 <br />111 <br />W120 <br />5 <br />20 <br />Chromium <br />5.10 <br />0.5 <br />5.000 <br />102 <br />w120 <br />9 <br />20 <br />Cobalt <br />5.06 <br />0.5 <br />5.000 <br />101 <br />80-120 <br />6 <br />20 <br />Copper <br />5.12 <br />0.5 <br />5.000 <br />102 <br />W120 <br />6 <br />20 <br />Lew <br />5.04 <br />1.0 <br />S. <br />101 <br />84120 <br />3 <br />20 <br />Wlybdenum <br />5.98 <br />0.5 <br />5.000 <br />Its <br />94120 <br />2 <br />20 <br />Nickel <br />5.18 <br />0.5 <br />5.000 <br />104 <br />94120 <br />4 <br />20 <br />Selenium <br />4.74 <br />0.5 <br />5.000 <br />95 <br />90-120 <br />5 <br />20 <br />Silva <br />5.93 <br />1.0 <br />3,000 <br />119 <br />W120 <br />0.9 <br />20 <br />71"itun <br />4.66 <br />0.5 <br />5.000 <br />93 <br />80- 120 <br />2 <br />20 <br />Vanadium <br />12.3 <br />0.5 <br />12.50 <br />99 <br />&G-120 <br />3 <br />20 <br />zinc <br />5.70 <br />0.5 <br />5.000 <br />114 <br />94120 <br />1 <br />20 <br />Mercury <br />1.26 <br />0.5 <br />1.250 <br />lot <br />94120 <br />0.6 <br />20 <br />Matrix Spilte (V 1) <br />Source. V9*U4-0 <br />Antimony <br />3.28 <br />0.5 mg/kg <br />5.000 <br />ND <br />66 <br />W120 QM -01 <br />Arsenic <br />5.64 <br />0.5 <br />5.000 <br />0.67 <br />99 <br />120 <br />Barium <br />45.8 <br />0.5 <br />12.50 <br />36.5 <br />74 <br />80- 120 QM -02 <br />Berylliurn <br />5.16 <br />0.5 <br />5,000 <br />ND <br />103 <br />84120 <br />Cadmium <br />5.45 <br />0.5 <br />5.000 <br />14D <br />109 <br />W120 <br />Chromium <br />15.7 <br />0.5 <br />5.000 <br />10.4 <br />106 <br />W120 <br />Cobalt <br />8.55 <br />0.5 <br />5.000 <br />4.20 <br />87 <br />84120 <br />Copper <br />14.1 <br />0.5 <br />5.000 <br />9.24 <br />its <br />84120 <br />Lead <br />7.56 <br />1.0 P <br />5.OW <br />2.39 <br />103 <br />W120 <br />Molybdenum <br />5,16 <br />0.5 <br />5.000 <br />ND <br />103 <br />wt20 <br />Nickel <br />11.3 <br />0.3 <br />5.000 <br />6.22 <br />101 <br />W120 <br />selenium <br />4.32 <br />0.5 <br />5.000 <br />ND <br />86 <br />W120 <br />Sam <br />5.76 <br />1.0 <br />5.000 <br />ND <br />Its <br />84120 <br />7hollium <br />4.93 <br />0.5 <br />5.000 <br />ND <br />99 <br />RNIZO <br />Vanadium <br />37.2 <br />0.5 <br />12.50 <br />24.9 <br />98 <br />80-120 <br />Zinc <br />24.7 <br />0.5 <br />5.000 <br />19.2 <br />Ito <br />W120 <br />Weary <br />1.33 <br />0.5 <br />1.250 <br />ND <br />106 <br />wt20 <br />ELUDE <br />