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110 2nd Avenue South #J)7 Pacheco CA 94553 5560 <br /> McCampbell Analytical, Inc. Telephone 925 798-1620 Fax 925 798-1622 <br /> Website www mccampbell corn F-mail marnCo)mccampbell Com <br /> QC SUMMARY REPORT FOR SW8015C <br /> ' W O Sample Matrix Soil QC Matrix Sad WorkOrder 0503163 <br /> EPA Method SW8015C Extraction SW3550C S1,1c1lD 15437 Spiked Sample ID 0503303-1102A <br /> ' Sample Spiked MS' MSD` MS-MSD' LCS LCSD LCS-LCSD Acceptance Criteria <br /> Analyte (%) <br /> mg/Kg mg/Kg %Rec %Rec %RPD %Rec % Rec %RPD MS I MSD LCS 1 LCSD <br /> TPH(d) 4 5 20 111 I 112 0 877 94 944 0 425 70- 130 70- 130 <br /> %SS 101 50 99 99 I 0 100 100 0 1 70- 130 70- 130 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions <br /> ' NONE <br /> BATCH 15437 SUMMARY <br /> ' Sample ID Date Sampled _ Date Extracted Date Analyzed Sample ID _ Date Sampled Date Extracted Date Analyzed <br /> 0503163-010A 3/08/05 3118105 11 59 AM 3119105 12 01 AM 0503163-012A 3108105 3118105 11 59 AM 3119105 4 34 AM ' <br /> 0503163-013A 3108/05 3118105 11 59 AM 3119/05 5 42 AM 0503163-016A 3!08105 3/18/05 11 59 AM 3/19/05 1 09 AM <br /> 0503163_011A 3/08/05 3118105 11 59 AM 3119105 2 17 AM 0503163-019A 3108105 3118105 11 59 AM 11191013 26 AM <br /> 1 <br /> MS=Matrix Spike MSD=Matrix Spike Duplicate LCS=Laboratory Control Sample LCSD=Laboratory Control Sample Duplicate RPD=Relative Percent Deviation <br /> %Recovery=100•(MS-Sample)!(Amount Spiked) RPD=100•(MS- MSD)1((MS+MSD)12) <br /> "MS I MSD spike recoveries and 1 or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons a)the sample is inhomogenous <br /> AND contains significant concentrations of analyte relative to the amount spiked or b)the spiked sample s matrix interferes with the spike recovery <br /> ' <br /> N/A=not enough sample to perform matrix spike and matnx spike duplicate <br /> NR=anal a concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content <br /> d <br /> HS Certification No 1644 -QA/QC Officer <br />