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it 0 2nd Avenue South #D7 Pacheco CA 94553-5560 <br /> L20 .__McCampbell Analytical hie Telephone 925-798 1620 Fax 925-798-1622 <br /> hnp I/www inccampbell com E mail niam@iiiccarripbell corn <br /> Advanced GeoEnvironmental, Inc Client Project ID Ripon Farm Service Date Sampled 01/02/03 <br /> 837 Shaw Road Date Received 01/03/03 <br /> ' Client Contact Bill Little Date Extracted 01/06/03-01/08103 <br /> Stockton, CA 95215 <br /> [Client P O Date Analyzed 01/06/03-01/08/03 <br /> Oxygenates and BTEX by GC/MS* <br /> Extraction Method SW5030B Analytical Method SW9260B Work Order 0301015 <br /> ' Lab ID 0301015-OOIB 0301015-002B 0301015-003B E 301015-004B <br /> ChentlD MW1/01-02-03 MW2/01-02-03 MW3/01-02-03 ! MW4/01-02-03 Reporting Limit for <br /> Matrix W W W W - DF=1 <br /> DF 1 1 1 10 SW <br /> l <br /> Compound Concentration ug/kg µg/L <br /> tert-Amyl methyl ether(TAME) ND ND ND ND<5 0 NA 05 <br /> Benzene ND 0 53 ND ND<5 0 NA 0 5 <br /> t-Butyl alcohol(TBA) 8 5 25 ND ND<50 NA 5 0 <br /> ' 1,2-Dibromoethane(EDB) ND ND ND ND<5 0 NA 05 <br /> 1 2-Dichloroethane(1,2-DCA) 15 18 ND 98 NA 05 <br /> Dmopropyl ether(D1PE) ND 0 55 ND ND<5 0 NA 0 5 <br /> Ethylbenzene ND ND ND ND<5 0 NA 05 <br /> Ethyl tert-butyl ether(ETRE) ND ND ND ND<5 0 NA 05 <br /> ' Methyl-t-butyl ether(MTBE) - ND 1 0 22 ND<5 0 NA 05 <br /> Toluene ND ND ND ND<5 0 NA 0 5 <br /> ' Xylenes ND ND 059 ND<5 0 NA 05 <br /> Surrogate Recoveries(%) <br /> ' %SSI 100 110 111 922 <br /> %SS2 102 101 968 104 <br /> %SS3 110 104 106 110 <br /> Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in gg/L,soil/sludge/solid samples in lig/kg, wipe samples inµg/vnpe, <br /> productloillnon-aqueous liquid samples in mg/L <br /> ' ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment j)sample diluted due to high <br /> organic content <br /> 1 <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />