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ydyLy <br /> ' <br /> � Mccamgbell Ana /cal, Inc. 1534 Willow Pass ROCusburg,CA 94565-1701 <br /> Web:wwwmccampbell.com E-mail:mainQmccarVhell.c= <br /> -When Ottality Caants" Tete hone:877-252-9262 Fax:925-252-9269 <br /> Baker Corp. Client Project ID: #198-263;Tuleburg Date Sampled: 09/30/10 <br /> 2700 California Avenue Warehouse Date Received: 09/30/10 <br /> Client Contact: Roland Grace Date Extracted: 09/30/10-10/01/10 <br /> Pittsburg,CA 94565 Client P.O.: Date Analyzed: 10/01/10 <br /> Volatile Organics by GC/MS(Basic Target hist)* <br /> Extraction Method: SW13ll(ZHETCLP)ISW5030B Analytical Method: SW9260B Work Order: 1009814 <br /> Lab ID 1009814-002A <br /> Client ID #2 <br /> Matrix Solid <br /> Conmound Concentration* DF Refoim;na Comnound Concentration* DF RC= <br /> i <br /> Acetone Q.g4 1.0 0, m 1 Mglbvl gther TAM 1.0 0,0005 <br /> B nz ne .0 0,0003, Bromobenzcne ND 1.0 0. <br /> r mochlorometha e ND 1.0 0.0005 Bromodichloromethaae I-0. Q. 0 <br /> Brouroform ND 1.0 m th n D 1-9 0.0005 <br /> tan a MEK 1.0 0.5 t-Butyl alcohol TB 1.0 010.5 <br /> n-Butyl benzene ND 1.0 0.0005 sec-Butv]benzene D 1.0 <br /> tert-Hut 1 benzene rb Disulfide ND 1.0 '0,00051 <br /> -Carbon Tetrachloride ND 1.0 0.00 Ch]Qroben4enD 1.0 0.000 <br /> Chloroethane ND 1.0 0.0005 Chloroform IM 1.0 0.000 <br /> Chloromethane 1.0 0.0005 -Chlorotoluen 1.0 0.000 <br /> 4-Chlorololuene ND 1.0 0 ibromochlorome 1.0 0.000 <br /> 1 2-Dibromo- - hl ro ro ane ND 1.0 10,0005 1.2-Dibromoethane1.0 0,0005 <br /> Dibromomethane1.0 0.0005 1.2-Dichlorobenzene ND 1.0 0.000 <br /> 1 -Dichlor z n 1. i hl r enzen 1.0 0.00051 <br /> Di t rodifluorome han 1.0 00005 1.1-DichloroelhaD 1-2 0.000 <br /> c l ord 1.0 0.0005 1.1-Dichloroethene ND 1.0 0.000 <br /> cis-12-Dichlor h n 1.0 0. trans-1 2-Dichlor D I.Q 0.000 <br /> 2-Dichloro ro ane ND 1.0 0.0005 1.3-Dichlororironane1.0 <br /> 01 <br /> 2.2-DichlOTonropane ND 1. -chloro ro ene ND <br /> 10 2.0go <br /> cis- ichl ene ND 1.0 0.0005 trans-] -Dic n 1-0 0,000 <br /> Diiso ro I ether DI 1.0 0,0005 Ethylbenzene 0.0022 1.0 0,00051 <br /> Ethyl Cert-butyl ether MTHEI ND 1.0 0.0005 Freon 113 ND 1 <br /> Hmic-hiorobutadiene ND J,0 .0= Hexachloroe h n J. .000 <br /> exanone 1.0 0.02 Isoprotw1benzenr NQ 1.0 <br /> 4-lsopropyl t l n 1.0 0. th 1-t-b l e 4 1.0 <br /> .010.00 <br /> /ene chlo 'de 1.0 Q.QO5 4-Me h 1-2- ntano M B 1.0 0. <br /> Noobthalene 1.0 l benzene 0.0029 <br /> 1.0 10.0005 <br /> Slwcne . 0.0005 1 J.I.2-Tetrachloroetbone ND 1.0 10,0005 <br /> ! 1.2.2-TetTachloroethane NID 1.0 0.0005 TctrachlproctheneD 1.0 <br /> 0.005 <br /> Toluene Q.QQ94 1.0 2 -Trichlorobenz 1.0 <br /> 0.0 <br /> 1 2 4-Trichlorobenzene ND 1.0 0.0 1 1-Trichloroelbanc. ND 1.0 0.000 <br /> ].1.2-Trichloroethgar ND 1.0 0,0905 Trichlororthene ND 1.0 0.005 <br /> TTichlorofluorometbane N2 1.0 0,0001 2 3-Tri hlor 1.0 0.0005 <br /> 1 2 4-Trimeth Ibenz t7 1.0 0. rimeth n 0.000 <br /> Surrogate Recoveries <br /> 93 % 2: 95 <br /> ° 76 <br /> Comments: <br /> "water and vapor samples are reported inµg/L,soil/sludge/solid samples in mg/kg,product/oil/non-aqueous liquid samples and all TCLP&SPLP extracts <br /> are reported in mg/L,wipe samples inµg/wipe. <br /> ND means not detected above the reporting limit/method detection limit;N/A means analyte not applicable to this analysis. <br /> #surrogate diluted out of range or surrogate coelutes with another peak;&)low/high surrogate recovery due to matrix interference. <br /> %SS=Percent Recovery of Surrogate Standard <br /> DF=Dilution Factor <br /> DHS ELAP Certification 1644 Angela Rydelius,Lab Manager <br />