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1 September 28 2004 P Lab ID STK436507 IGround Zero Analysis Customer 3-14996 Quality Control - Organic Constituent Method Date/ID Type Units Cone QC Data D O Note 1 1 1 2-Tetrachloroethane 5242 09/20/2004 A209 BS ug/L 1000 93 0% 77-138 BSD ug/L 1000 103% 77-138 BSRPD ug/L 104% :515 8 5242 09/20/2004 A 00-CCV ug/L 1000 969% 70-130 1 1 2,2-Tetrachloroethane 5242 09/20/2004 A209 Blank ug/L ND <05 BS ug/L 1000 94 8% 79-147 BSD ug/L 1000 105% 79-147 BSRPD ug/L 99% 525 9 5242 09/20/2004 A 00-CCV ug/L 1000 97 2% 70-130 Tetrachloroethylene 5242 09/20/2004 A209 Blank ug/L ND <05 BS ug/L 1000 866% 71-136 BSD ug/L 1000 845% 71-136 BSRPD ug/L 25% 514 7 I 5242 09/20/2004 A 00-CCV ug/L 1000 85 1% 70-130 Toluene 5242 09/20/2004 A209 Blank ug/L ND <05 BS ug/L 1000 83 6% 78-126 BSD ug/L 1000 2 5% 78 BSRPD ug/L 2 3% 5 16 16 4 4 5242 09/20/2004 A 00-CCV ug/L 1000 869% 70-130 ' 1,2 3-Tnchlorobenzene 5242 09/20/2004 A209 Blank ug/L ND <0 5 BS ug/L 1000 115% 74-151 BSD ug/L 1000 134% 74-151 BSRPD ug/L 155% S 2 5 4 ' 5242 09/20/2004 A 00-CCV ug/L 1000 108! 70-130 1 2 4-Trtchlorobenzene 5242 09/20/2004 A209 Blank ug/L ND <05 BS ug/L 1000 111% 74-152 ' BSD ug/L 1000 123% 74-152 BSRPD uglL 10 8% 5 21 7 524 2 09/20/2004 A 00-CCV ug/L 1000 105% 70-130 ' 1 1 1-Trichloroethane 5242 09/20/2004 A209 Blank ug/L ND <0 5 BS ug/L 1000 101% 84-144 BSD ug/L 1000 105% 84-144 BSRPD ug/L 3 8% 517 8 ' 5242 09/20/2004 A 00-CCV ug/L 1000 101% 70-130 1,1 2-Trichloroethane 5242 09/20/2004 A209 Blank ug/L ND <05 BS ug/L 1000 879% 80-132 BSD ug/L 1000 104% 80-132 BSRPD ug/L 16 9% -.5200 524 2 09/20/2004 A 00-CCV ug/L 1000 87 8% 70-130 Tru hloroethylene 524 2 09/20/2004 A209 Blank ug/L ND <0 5 Report continued on next page STK436507 Quality Control Page 7 I