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September 28, 2004 Lab ID STK436504 ' Ground Zero Analysts Customer 3-14996 Quality Control - Organic ' =Constituent Method Date/ID Type Units Conc QC Data DQO Note n-Butylbenzene 5242 09/20/2004 A209 BS ug/L 1000 834% 89-158 435 ' BSD ug/L 1000 83 1% 89-158 435 BSRPD ug/L 04% 515 3 5242 09/20/2004 A 00-CCV ug/L 1000 85 4% 70-130 sec-Butylbenzene 5242 09/20/2004 A209 Blank ug/L ND <0 5 BS ug/L 1000 80 6% 92-147 435 BSD uglL 1000 799% 92-I47 435 ' BSRPD ug/L 0 8% 515 3 524 2 09/20/2004 A 00-CCV ug/L 1000 83 4% 70-130 cert-Butylbenzene 5242 09/20/2004 A209 Blank ug/L ND <05 ' BS uglL 1000 78 7-% 79-140 BSD ug/L 1000 797% 79-140 BSRPD ug/L 13% 515 8 ' 5242 09/20/2004 A 00-CCV ug/L 1000 81 3% 70-130 Carbon Tetrachloride 5242 09/20/2004 A209 Blank uglL ND <05 BS ug/L 1000 103% 80-151 BSD ug/L 1000 108% 80-151 BSRPD ug/L 4 8% 520 6 5242 09/2012004 A 00-CCV ug/L 1000 102% 70-130 ' Chlorobenzene 5242 09/20/2004 A209 Blank ug/L ND <0 5 BS ug/L 1000 845% 74-134 BSD ug/L 10 00 879% 74-134 BSRPD ug/L 40% 5 16 9 ' 524 2 09/20/2004 A 00-CCV ug/L 1000 850% 70-130 Chloroethane 5242 09/20/2004 A209 Blank ug1L ND <0 5 BS uglL 1000 101% 80-173 ' BSD ug/L 1000 998% 80-173 BSRPD ug/L 0 8170 516 1 I 524 2 09/20/2004 A 00-CCV ug/L 1000 940% 70-130 ' Chloroform 524 2 09/20/2004 A209 Blank ug/L ND <05 BS ug/L 1000 94 1% 78-141 BSD ug/L 1000 104% 78-I41 BSRPD uglL 101% 5176 5242 09/20/2004 A 00-CCV ug/L 1000 93 1% 70-130 Chloromethane 5242 09/20/2004 A209 Blank ug/L ND <05 BS ug/L 1000 129% 68-165 BSD ug/L 1000 115% 68-165 BSRPD ug/L 11 6% 515 7 524 2 1 09/20/2004 A 00-CCV ug/L 1 1000 103% 70-130 2-Chiorotoluene 524 2 09/20/2004 A209 Blank ug/L ND <0 5 Report continued on next page STK436504 Quality Control Page 2 f