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July 16, 2004 Lab ID SP 406527 ' Ground Zero Analysis Customer 3-14996 Quality Control - Organic ' Constituent Method Date/ID Type Units Conc QC Data D O Note ' Hexachlorobutadtene 5242 07/07/2004 A209 BS ug/L 1000 95 8% 73-154 BSB ug/L 1000 97 1% 73-154 BSRPD ug/L 13% 515 8 ' 5242 07/07/2004 A 00-CCV ug/L 1000 120% 70-130 lsopropylbenzene 5242 07/07/2004 A209 Blank ug/L ND <0 5 BS ug/L 1000 996% 88-143 ' BSD ug/L 1000 88 8% 88-143 BSRPD ug/L 09% 517 0 5242 07/07/2004 A 00-CCV ug/L 1000 106% 70-130 ' p-Isopropyltoluene 5242 07/07/2004 A209 Blank ug/L ND <0 5 BS ug/L 1000 940% 88-153 SSD ug/L 1000 907% 88-153 BSRPD ug/L 3 6% 1 514 8 ' 5242 07/07/2004 A 00-CCV ug/L 10 00 117% 70-130 Methyl ten-Butyl Ether (MTBE) 5242 07/07/2004 A209 Blank ug/L ND <1 BS ug/L 10 00 104% 62-143 BSD ug/L 10 00 972% 62-143 BSRPD ug/L 67% 517 6 5242 07/07/2004 A 00-CCV ug/L 1000 890% 70-130 ' Naphthalene 5242 07/07/2004 A209 Blank ug/L ND <05 BS ug/L 1000 120% 63-165 BSD ug/L 1000 108% 63-165 BSRPD ug/L 107% :530 6 5242 07/07/2004 A 00-CCV ug/L 10 00 125% 70-I30 n-Propylbenzene 5242 07/07/2004 A209 Blank ug/L ND <0 5 ' BS ug/L 1000 880% 85-152 BSD ug/L 1000 88 7% 85-152 BSRPD ug/L 07% 515 6 5242 07/07/2004 A 00-CCV ug/L 10 00 107% 70-130 ' Styrene 5242 07/07/2004 A209 Blank ug/L ND <05 BS ug/L 1000 920% 85-149 BSD ug/L 1000 85 7% 85-149 ' BSRPD ug/L 7 1% 5 16 8 524 2 07/07/2004 A 00-CCV ug/L 1000 109% 70-130 Tert-amyl methyl Ether (TAME) 524 2 07/07/2004 A209 Blank ug/L ND <3 ' 13S ug/L 1000 93 4% 67-129 BSD ug/L 1000 816% 67-129 BSRPD Ug/L 1 2 53 00 5242 07/07/2004 A 00-CCV ug/L 1000 84 9% 70-130 1 1 1 2-Tetrachloroethane 5242 07/07/2004 A209 Blank ug/L ND <0 5 Report continued on next page SP 406527 Quality Control Page 6