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1 July 16, 2004 Lab ID SP 406523 ' Ground Zero Analysis Customer 3-14996 Quality Control - Organic r =Constituent Method Date/ID Type Units Conc QC Data DQO Note ' n-Butylbenzene 5242 07/02/2004 A209 BS ug/L 1000 94 2% 89-158 BSD ug/L 1000 115% 89-158 BSRPD ug/L 19 6% 515 3 410 5242 07/02/2004 A 00-CCV ug/L 1000 103% 70-130 ' sec-Butylbenzene 5242 07/02/2004 A209 Blank ug/L ND <05 BS ug/L i0 00 92 7% 92-147 BSD ug/L 1000 108% 92-147 ' BSRPD ug/L 154% 515 3 410 5242 07/02/2004 A 00-CCV ug/L 10 00 104% 70-130 ' tert-Butylbenzene 5242 07/02/2004 A209 Blank ug/L ND <05 BS ug/L 1000 97 1% 79-140 BSD ug/L 1000 109% 79-140 BSRPD ug/L 117% 515 8 ' 5242 07/02/2004 A 00-CCV ug/L 10 00 102% 70-130 Carbon Tetrachloride 5242 07/02/2004 A209 Blank ug/L ND <0 5 BS ug/L 1000 864% 80-151 BSD ug/L 1000 105% 80-151 BSRPD ug/L 190% 520 6 5242 07/02/2004 A 00 CCV ug/L 1000 92 9% 70-130 ' Chlorobenzene 5242 07/02/2004 A209 Blank ug/L ND <0 5 BS ug/L 1000 88 2% 74-134 BSD ug/L 10 00 88 0% 74-134 BSRPD ug/L 03% 516 9 ' 5242 07/02/2004 A oo-CCV ug/L 1000 91 1% 70-130 Chloroethane 5242 07/02/2004 A209 Blank ug/L ND <0 5 B3 ug/L 1000 899% 80-173 ' BSD ug/L 1000 106% 80-173 BSRPD ug/L 167% 516 1 410 524 2 07/02/2004 A 00-CCV ug/L 10 00 859% 70-130 r Chloroform 5242 07/02/2004 A209 Blank ug/L ND <05 BS ug/L 1000 106% 78-141 BSD ug/L 1000 910% 78-141 BSRPD ug/L 15 6% 517 6 r5242 07/02/2004 A 00 CCV ug/L 1000 103% 70-130 Chloromethane 524 2 07/02/2004 A209 Blank ug/L ND <05 r BS ug/L 1000 925% 68-165 BSD ug/L 10 00 117% 68-165 BSRPD ug/L 232% 515 7 410 524 2 07/02/2004 A 00-CCV ug/L 1000 83 5% 70-130 2-Chlorotoluene 524 2 07/02/2004 A209 tank ug/L ND <0 5 ' Report continued on next page ' SP 406523 Quality Control Page 2 r