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RECEIVED <br /> A N A L Y T I C A L ��� 0199a <br /> LABORATORIES <br /> Certificate of Analysis <br /> John Lane <br /> Ground Zero Preparation Date 11/20/98 <br /> 1719 Main Street Analysts Date 11/20/98 <br /> Escalon, CA 95320- Report Issue Date 11/25/98 <br /> Sample Date 11/09/98 <br /> Submission Number 9811CCO298 Sample Time 1656 <br /> Lab Number 85892 Sample Type SOLID <br /> Project Number 263 <br /> Project Desc Tubburg Warehouse <br /> Sample Description TW-1A <br /> Oxygenates by GC/MS (8260M) <br /> Analyte Result Units PQL DtI DLR <br /> Methyl-t-Butyl Ether 420 µg/Kg 20 5 100 <br /> Di-isopropyl Ether ND µg/Kg 20 1 20 <br /> Ethyl t-Butyl Ether ND µg/Kg 20 1 20 <br /> t-Amyl Methyl Ether ND ag/Kg 20 1 20 <br /> tert-Butyl Alcohol 1600 µg/Kg 200 S 1000 <br /> ND None Detected PCL Pra,-rlLal Quantitation Limit Conversions <br /> mg/L Milligrams/Liter = ppm DiI Dilution Factor 1 ppm = 1000 ppb <br /> Pg/L Micrograms/Liter = ppb DLR Reportable Detection Limit 1 ppb = 0 001 ppm a <br /> ma llrltlligrams/kilogram = ppm Trwed by (PQL e Dcl) <br /> P Micrograms/Kilogram = ppb Higher limits may result from exceptional sample matrices or interterenc.La <br /> 1414 Stanislaus Street + Fresno, CA 93706-1623 Phone 209-497-2888, In CA 800-877-8310 + Fax 209-485-6935 <br />