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A N A L Y T I C A L <br /> LABORATORIES <br /> Certificate of Analysis <br /> John Lane <br /> Ground Zero Preparation Date 11/20/98 <br /> 1714 Main Street Analysis Date 11/20/98 <br /> Escalon, CA 95320- Report Issue Date 11/25/98 <br /> Sample Date 11/10/98 <br /> Submission Number 9811000298 Sample Time 1244 <br /> Lab Number 85897 Sample Type SOLID <br /> Project Number 263 <br /> Project Desc Tubburg Warehouse <br /> Sample Description. TW-6A <br /> Oxygenates by GC/MS 8260M <br /> Analyte Result Units PQL Dil DLR <br /> Methyl-t-Butyl Ether 1600 pg/Kg 20 5 100 <br /> Di-isopropyl Ether N`D 14g/Kg 20 5 100 <br /> Ethyl t-Butyl Ether ND ug/Kg 20 5 100 <br /> t-Amyl Methyl Ether ND ;eg/Kg 20 5 100 <br /> tert-Butyl Alcohol 1100 Ag/Kg 200 5 1000 <br /> ND None Detected P -)L Prictiial Quantitation Lima Conversions <br /> mg/L Milligrams/Liter ppm D, Dilution Factor 1 ppm = 1000 ppb <br /> �y/L 1Vlicrosrams/Liter — ppb DLR R.poriable Detection Limit 1 ppb = 0 001 ppm <br /> mg/k- IVlilligrams/Kilogram — ppm deri4zd by (PQL e Di1) <br /> Kg/ Micrograms/Kilogram — ppb Higher limits may result from exceptional sample matrices or interferences <br /> 1414 Stanislaus Street • Fresno, CA 93706-1623 • Phone 209-497-2888, In CA 800-877-8310 • Fax 209-485-6935 <br />