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II <br /> GeoAnalytical Laboratories, Inc. <br /> 2300 Maryann Dr. Turlock,CA 95380 Phone(209)669-0100 Fax(209)668-8516 <br /> email: lab.geo@att.net <br /> Report# V9110608 Project: Morada Tank Pull, Date:08/19/09 <br /> Jim Thorpe,Inc. Date Recd:08/06/09 <br /> PO Box 357 PO# <br /> Lodi,CA 95241 <br /> CERTIFICATE OF ANALYSIS Date Sampled: 08/06/09 <br /> Sampler: Steven Heune <br /> Sample ID Time: Lab 1D RL Method Analyte Result Units Notes Started <br /> Dispenser 13:20 V91-10608-17 5.0 8260B 1,2-Dichloroethane ND ug/kg 8/10/09 10:41 am. <br /> 10.0 Di-isopropyl Ether(DIPE) ND <br /> 400 Ethanol ND <br /> 10.0 Ethyl ten-Butyl Ether(ETBE) ND <br /> 10.0 Ethylene dibromide ND <br /> 10.0 Methyl tert-Butyl Ether(MTBE) ND <br /> 10.0 Tert-Amyl Methyl Ether(TAME) ND <br /> 200 tert=Butanol(TBA) ND <br /> 1.0 GC/MS Gasoline ND mg/kg <br /> Sample Notes Surrogate Amnt Spiked Amnt Recovered %Recovery QC Limit% Surrogate Notes <br /> 1,2-Dichloroethane-d4 20.00. 21.8 109% 66-133 <br /> 2-Bromo-l-Chloropropane 20.00 22.8 114% 63-139 <br /> 4-Bromofluorobenzene 20.00 20.1 101% 64-136 <br /> Dispenser 13:25 V91-10608-18 5.0 8260B 1,2-Dichloroethane ND ug/kg 8/10/09 10:41 am <br /> 10.0 Di-isopropyl Ether(DIPE) ND <br /> 400 Ethanol ND <br /> 10.0 Ethyl tert-Butyl Ether(ETBE) ND <br /> 10.0 Ethylene dibromide ND <br /> 10.0 Methyl tert Butyl Ether(MTBE) ND <br /> 10.0 Tert-Amyl Methyl Ether(TAME) ND <br /> 200 tert-Butanol(TBA) ND <br /> 1.0 GC/MS Gasoline ND mg/kg <br /> Sample Notes Surrogate Amur Spiked Amnt Recovered %Recovery QC Limit% Surrogate Notes <br /> 1,2-Dichloroethane-d4 20.00 23.3 117% 66-133 <br /> 2-Bromo-I-Chloropropane 20.00 24.8 124% 63-139 <br /> 4-Bromofluorobenzene 20.00 20.3 101% 64-136 <br /> Piping 1 13:30 V9H0608-19 5.0 8260B 1,2-Dichloroethane ND ug/kg 8/10/09 10:41 am <br /> 10.0 - Di-isopropyl Ether(DIPE) ND <br /> 400 Ethanol ND <br /> 10.0 Ethyl tert-Butyl Ether(ETBE) ND <br /> 10.0 Ethylene dibromide ND <br /> 10.0 Methyl tert--Butyl Ether(MTBE) ND <br /> 10.0 Tert-Amyl Methyl Ether(TAME) ND <br /> 200 tert-Butanol(TBA) ND <br /> 1.0 GC/MS Gasoline ND mg/kg <br /> Sample Notes Surrogate Amnt Spiked Amnt Recovered %Recovery QC Limit% Surrogate Notes <br /> 1,2•Dichloroethane-d4 20.00 23.3 117% 66-133 <br /> 2-Bromo-1-Chloropropane 20.00 23.8 119% 63-139 <br /> 4-Bromofluorobenzene 20.00 20.4 102%, 64-136 <br /> Mario D'Onofrio Richard Sereno <br /> Chemist Quality Assurance Officer <br /> Certification#2585 <br />