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COLUMBIA ANALYTICAL SERVICES,INC <br /> Analytical Report <br /> Client EMCON Associates Service Request- S941442 <br /> Protect Federated-Frank's Exxon/25 20-100 01 Date Collected 11/14/94 <br /> Sample Matrix Water Date Received 11/15/94 <br /> Date Extracted 11/16,22/94 <br /> Date Analyzed 11/17-24194 <br /> TPH as Diesel <br /> EPA Method 3510/California DHS LUFI'Method <br /> Units ug/L. (ppb) <br /> Sample Name Lab Code MRL Result <br /> MW-1 5941442-001 50 ND <br /> MW-2 S941442-002 50 100 <br /> MW-3 5941442-003 50 ND <br /> MW4 S941442-004 50 1,900 ** <br /> Method Blank S941116-WB 50 ND <br /> Method Blank 5941122-WB 50 ND <br /> * This sample contains a higher boiling point hydrocarbon mixture,quantified as diesel The chromatogram does not <br /> match the typical diescl fingerprint <br /> ** This sample contains a mixture of lower and higher boiling point hydrocarbons, quantified as diesel The <br /> chromatogram does not match the typical diesel fingerprint <br /> Approved By ` Date ffr",-- r4o� <br /> IAMRIJ060194 <br /> Page 3 of 9 <br /> 1921 Ringwood Avenue • Son Jose California 95131 • Telephone 408/437 2400 0 Fox 408/437 9356 <br />