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Spargero Analytical LaboratoryDivl Division <br /> Technolog - Mobile Laboratory DpAslon <br /> y inc Scientific Dmision <br /> With Automation in Mind <br /> EPA Method 601 <br /> Halogenated Volatile Organics Laboratory Control Spike (LCS) <br /> and Laboratory Control Spike Duplicate (LCSD) <br /> Attention Mr Jeff Rothgery Date Sampled Nov 27, 1996 <br /> Apex Envirotech, Inc Date Received Nov 29, 1996 <br /> 7844 Madison Ave , Ste 106 Date Analyzed Dec 4, 1996 <br /> Fair Oaks, CA 95628 Invoice# 7247 <br /> Project# ERA02 009 Project Name Moore Petroleum <br /> Client ID LCS/LCSD LAB ID 7247-LCS <br /> 7247-LCSD <br /> Matrix Water Dilution <br /> UNITS= augtl <br /> Sample Spike Spike Dup Spike Dup QC Limits <br /> Compound Conc Added Result Result % Rec % Rec RPD RPD % Rec <br /> 1,1-D(chloroethane ND 10 90 90 90% 90% 0% 20 65-135 <br /> Trichloroethene ND 10 80 80 80% 80% 0% 20 65-135 <br /> 1,2-Dichloropropane ND 10 90 80 90% 80% 12% 20 65-135 <br /> Chlorobenzene ND 10 80 80 80% 80% 0% 20 65-135 <br /> 1,2-Dichlorobenzene ND 10 80 70 80% 70% 13% 20 65-135 <br /> Surrogate % Recovery of 2-Bromo-l-Chloropropane= 84% LCS 88% LCSD <br /> Surrogate % Recovery of 1,4-Dichlorobutane= 80% LCS 79% LCSD <br /> ppb=parts per billion=ugA=micrograms per liter <br /> ppm=parts per million=uglml=micrograms per millilder <br /> ND=Not Detected Compound(s)maybe present at concentrations below the detection limit <br /> Dec 20, 1996 <br /> Ft L James,Principal Chemist• Hate Reported SPARGER TECHNOLOGY ANALYTICAL LABORATORY INC IS CERTIFIED BY THE STATE OF CALIFORNIA <br /> DEPARTMENT OF HEALTH SERVICES AS A HAZARDOUS WASTE TESTING LABORATORY <br /> (Certsricabon No 1614) <br /> 601 LCSW XLS <br /> 3050 Fite Circle, Suite 112 - Sacramento California 95827 • (996) 362-8947 • FAX(996) 362-0947 <br />