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Wiil L <br />Client: Union Pacific Rail Road - <br />Project Name: <br />Weck Laboratories, Inc. <br />Environmental and Analytical Services - Since 1964 <br />Report Date: Thursday, April 20, 2000 <br />CERTIFICATE OF ANALYSIS <br />Lab#: A002448-001 Sample <br />Sampled By: Jack Dishman <br />Parameter <br />ID: STKN Sludge <br />Date: 3/31/00 <br />Result <br />Time: 13:32 <br />Units <br />Dilution <br />Factor <br />Matrix: <br />RL <br />Sludge <br />Method <br />Analyzed <br />Worksheet # <br />Soluble silver on WET extract (STLC) <br />ND <br />mg/L <br />1 <br />0.02 <br />EPA 6020 <br />4/14/00 at <br />WS13316 <br />Soluble thallium on WET extract (STLC) <br />ND <br />mg/L <br />1 <br />0.05 <br />EPA 6020 <br />4/14/00 at <br />WS13316 <br />Solule vanadium on WET extract (STLC <br />ND <br />mg/L <br />1 <br />0.20 <br />EPA 6020 <br />4/14/00 at <br />WS13316 <br />Soluble zinc on WET extract (STLC) <br />1.8 <br />mg/L <br />1 <br />0.50 <br />EPA 6020 <br />4/14/00 at <br />WS13316 <br />Flash point <br />>200 <br />Deg. F <br />1 <br />EPA 1010 <br />4/19/00 sl <br />WS13457 <br />Fish Bioassay <br />> 750 <br />mg/L <br />1 <br />Sub -contract <br />4/7/00 to <br />WS13448 <br />Mercury <br />ND <br />mg/L <br />1 <br />0.002 <br />EPA 245.1 <br />4/6/00 kk <br />WS13039 <br />pH <br />5.90 <br />Units <br />1 <br />SM 4500 H B <br />4/4/00 aw <br />WS13049 <br />Soluble Mercury in STLC <br />ND <br />mg/L <br />1 <br />0.006 <br />EPA 7471 <br />4/14/00 kk <br />WS13351 <br />Lab#: A002448-002 Sample <br />ID: STKN Waste Oil <br />Matrix: <br />Sludge <br />Sampled By: Jack Dishman <br />ate: 3/31/00 Time: 14:00 <br />Dilution <br />Parameter <br />Result <br />Units <br />Factor <br />RL <br />Method <br />Analyzed <br />Worksheet # <br />Fish Bioassay <br />612 <br />mg/L <br />1 <br />Sub -contract <br />4/7/00 to <br />WS 13448 <br />pH (10X leach) <br />6.3 <br />Units <br />1 <br />EPA 9045M <br />4/20/00 kk <br />WS 13480 <br />Total Releasable Hydrogen Sulfide <br />ND <br />mg/kg <br />1 <br />10.0 <br />SW846 s7.3.4 <br />4/19/00 tc <br />WS13473 <br />Flash point <br />>200 <br />Deg. F <br />1 <br />EPA 1010 <br />4/7/00 aw <br />WS13274 <br />� <br />Dr c k:&Z'- <br />Y.% <br />Notes: <br />J PAhorized <br />Signature <br />Any remaining sample(s) for testing will <br />a disposed of one month from the final report date <br />unless other <br />arrangements <br />are made in advance. <br />All results are expressed on wet weight <br />basis unless specified. <br />RL = Reporting Limit. <br />ND = Not detected above the reporting ii <br />it. <br />ELAP # 1132 <br />TR = Trace detection, detected but below <br />the RL. <br />LACSD # 10143 <br />J = Estimated value, detected but below <br />the RL. <br />H = Estimated value, result is over thelibration <br />range. <br />Sub = Subcontracted analysis, original r <br />port enclosed. <br />Lab#: A002448 Page 2 of 2 <br />14859 East Clark Avenue, City of Industry, California 91745-1396 (626) 336-2139 FAX (626) 336-2634 <br />www.wecklabs.com <br />