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W11 L Weck Laboratories, Inc. Environmental and Analytical Services - Since 1964 Client: Union Pacific Rail Road - Sto kton QC Report Date: Thursday, April 20, 2000 Project Name: 4/14/00 Auble metals on stic (WET) by ICP -MS Project #: QUALITY CONTROL REPORT Amt. 01 RPD Sample QC Added/ True for Low High %R or 9 QC Lab# TestGroup Para eter Result Result Units Value RPD MSD Limit Limit Method Blank 6020_stic Solub a cobalt on WET extract (STLC) 0.00 mg/L Method Blank 6020_stic Solub e copper on WET extract (STLC) 0.00 mg/L Method Blank 6020_stic Solub e lead on WET extract (STLC) 0.00 mg/L Method Blank 6020_stic Solub e molybdenum on WET extract (STLC) 0.00 mg/L Method Blank 6020_stic Solub nickel on WET extract (STLC) 0.00 mg/L Method Blank 6020_stic Solubl selenium on WET extract (STLC) 0.00 mg/L Method Blank 6020_stic Solubl silver on WET extract (STLC) 0.00 mg/L Method Blank 6020_stic Solubl thallium on WET extract (STLC) 0.00 mg/L Method Blank 6020 stic Solubl total chromium on WET ext.-STLC 0.00 mg/L Method Blank 6020_stic Solubl zinc on WET extract (STLC) 0.00 mg/L Method Blank 6020_stic Solute vanadium on WET extract (STLC) 0.00 mg/L QCS 6020_stic Solubl antimony on WET extract (STLC) 0.05 mg/L 0.05 96 QCS 6020_stic Solubl arsenic on WET extract (STLC) 0.05 mg/L 0.05 94 QCS 6020_stic Solubl barium on WET extract (STLC) 0.05 mg/L 0.05 98 QCS 6020_stic Solubl beryllium on WET extract (STLC) 0.05 mg/L 0.05 96 QCS 6020_stic Solubl cadmium on WET extract (STLC) 0.05 mg/L 0.05 102 QCS 6020_stic Solubl cobalt on WET extract (STLC) 0.05 mg/L 0.05 96 QCS 6020_stic Solubl copper on WET extract (STLC) 0.05 mg/L 0.05 96 QCS 6020_stic Solubl lead on WET extract (STLC) 0.05 mg/L 0.05 100 QCS 6020_stic Solubl molybdenum on WET extract (STLC) 0.05 mg/L 0.05 98 QCS 6020_stic Solubl nickel on WET extract (STLC) 0.05 mg/L 0.05 92 QCS 6020_stic Solubl selenium on WET extract (STLC) 0.05 mg/L 0.05 94 QCS 6020_stic Soluble silver on WET extract (STLC) 0.05 mg/L 0.05 98 QCS 6020_stic Soluble thallium on WET extract (STLC) 0.05 mg/L 0.05 102 QCS 6020_stic Soluble total chromium on WET ext.-STLC 0.05 mg/L 0.05 98 QCS 6020_stic Soluble zinc on WET extract (STLC) 0.05 mg/L 0.05 94 QCS 6020_stic Solule anadium on WET extract (STLC) 0.05 mg/L 0.05 96 Worksheet #: WS13316 WS13316 WS13316 WS13316 Note: ND = Not Detected BL = Blank Lab#: A002447-001 A002448-001 A002570-001 A002577-001 3st Name Analyzed Date Auble metals on stic (WET) by ICP -MS 4/14/00 )luble metals on stic (WET) by ICP -MS 4/14/00 Auble metals on stic (WET) by ICP -MS 4/14/00 Auble metals on stic (WET) by ICP -MS 4/14/00 MS = Matrix Spike MSD = Matrix Spike Duplicate SURR = Surrogate DUP = Duplicate RPD = Relative Percent Deviation LCS = Laboratory Control Standard Page 11 of 15 14859 East Clark Avenue, City f Industry, California 91745-1396 (626) 336-2139 FAX (626) 336-2634 www.wecklabs.com