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QC Sample Results <br />Client: ARCADIS U.S. Inc TestAmerica Job ID: 720-69888-1 <br />ProjecUSite: UPRR-Stockton <br />Method: 8260B - Volatile prganic Compounds (GC/MS) (Continued) <br />Lab Sample ID: LCSD 720-19 <br />142/6 <br />Client <br />Sample ID: Lab <br />Control <br />Sample <br />Dup <br />Matrix: Solid <br />Prep Type: Total/NA <br />Analysis Batch: 196186 <br />Prep Type: Total/NA <br />Analysis Batch: 196142 <br />Prep Batch: 196071 <br />MB MB <br />Analyte <br />Result Qualifier <br />Spike <br />LCSD <br />LCSD <br />Antimony <br />%Rec. <br />ND <br />RPD <br />Analyte <br />01/22/1612:56 01/25/1613:48 1 <br />Added <br />Result <br />Qualifier Unit <br />D •/ Rec <br />Limits <br />RPD <br />Limit <br />--- -- <br />cis- 1,3-Dichloropropene <br />ND <br />5000 <br />5410 <br />--- --- <br />ug/Kg <br />108 <br />79-144 <br />0 <br />20 <br />trans -l,3-Dichloropropene <br />5000 <br />5510 <br />ug/Kg <br />110 <br />78-144 <br />0 <br />20 <br />Ethylbenzene <br />5000 <br />587D <br />ug/Kg <br />117 <br />76-137 <br />0 <br />20 <br />Hexachlorobutadiene <br />5000 <br />5440 <br />ug/Kg <br />109 <br />63-150 <br />0 <br />20 <br />2-Hexanone <br />20000 <br />21800 <br />ug/Kg <br />109 <br />54-124 <br />0 <br />20 <br />Isopropylbenzene <br />5000 <br />5470 <br />ug/Kg <br />109 <br />65-128 <br />1 <br />20 <br />4-Isopropyltoluene <br />5000 <br />5820 <br />ug/Kg <br />116 <br />62-153 <br />0 <br />20 <br />Methylene Chloride <br />5000 <br />5310 <br />ug/Kg <br />106 <br />70-130 <br />7 <br />20 <br />4-Methyl-2-pentanone(MIBK) <br />20000 <br />21900 <br />ug/Kg <br />109 <br />53-129 <br />3 <br />20 <br />Naphthalene <br />5000 <br />4990 <br />ug/Kg <br />100 <br />62-151 <br />1 <br />20 <br />N-Propylbenzene <br />5000 <br />5570 <br />ug/Kg <br />111 <br />65-144 <br />1 <br />20 <br />Styrene <br />5000 <br />5100 <br />ug/Kg <br />102 <br />79-139 <br />0 <br />20 <br />1,1,1,2 -Tetrachloroethane <br />5000 <br />5490 <br />ug/Kg <br />110 <br />72-129 <br />2 <br />20 <br />1,1,2,2 -Tetrachloroethane <br />5000 <br />5200 <br />ug/Kg <br />104 <br />69-133 <br />4 <br />20 <br />Tetrachloroethene <br />5000 <br />5440 <br />ug/Kg <br />109 <br />79-130 <br />1 <br />20 <br />Toluene <br />5000 <br />5520 <br />ug/Kg <br />110 <br />77-120 <br />1 <br />20 <br />1,2,3-Tdchlorobenzene <br />5000 <br />5330 <br />ug/Kg <br />107 <br />72-159 <br />1 <br />20 <br />1,2,4-Trichlorobenzene <br />5000 <br />5830 <br />ug/Kg <br />117 <br />71-163 <br />2 <br />20 <br />1,1,1 -Trichloroethane <br />5000 <br />5600 <br />ug/Kg <br />112 <br />69-132 <br />0 <br />20 <br />1,1,2 -Trichloroethane <br />5000 <br />5580 <br />ug/Kg <br />112 <br />70-130 <br />1 <br />20 <br />Trichloroethene <br />5000 <br />5610 <br />ug/Kg <br />112 <br />69-129 <br />0 <br />20 <br />Trichlorofluoromethane <br />5000 <br />5360 <br />ug/Kg <br />107 <br />49-140 <br />2 <br />20 <br />1,2,3-Trichloropropane <br />5000 <br />5190 <br />ug/Kg <br />104 <br />74-135 <br />3 <br />20 <br />1,1,2-Trichloro-1,2,2-tdfiuoroetha <br />5000 <br />5570 <br />ug/Kg <br />111 <br />66-128 <br />1 <br />20 <br />ne <br />1,2,4-Trimethylbenzene <br />5000 <br />5330 <br />ug/Kg <br />107 <br />62-155 <br />0 <br />20 <br />1,3,5-Trimethyibenzene <br />5000 <br />5240 <br />ug/Kg <br />105 <br />69-142 <br />2 <br />20 <br />Vinyl acetate <br />5000 <br />5360 <br />ug/Kg <br />107 <br />56-200 <br />4 <br />20 <br />Vinyl chloride <br />5000 <br />3370 <br />ug/Kg <br />67 <br />10-118 <br />11 <br />20 <br />m -Xylene 8 p -Xylene <br />5000 <br />5840 <br />ug/Kg <br />117 <br />71-142 <br />0 <br />20 <br />o -Xylene <br />5000 <br />5580 <br />ug/Kg <br />112 <br />71-142 <br />1 <br />20 <br />2,2-Dichloropropane <br />5000 <br />5310 <br />ug/Kg <br />106 <br />67-146 <br />5 <br />20 <br />LCSD LCSD <br />S -98M <br />vwy Qualifier <br />Limits <br />4-BromoBuoobenzene <br />118 <br />66-148 <br />1,2-Dichloroethane-d4 (Surr) <br />119 <br />62-137 <br />Toluene -d8 (Surr) <br />117 <br />65-141 <br />Method: 6010B - Metals (NCP) <br />Lab Sample ID: MB 720-1960 <br />111-A <br />Client Sample ID: Method Blank <br />Matrix: Solid <br />Prep Type: Total/NA <br />Analysis Batch: 196186 <br />Prep Batch: 196071 <br />MB MB <br />Analyte <br />Result Qualifier <br />RL <br />MDL Unit <br />D Prepared Analyzed DII Fac <br />Antimony <br />ND <br />0.50 <br />0.083 mg/Kg <br />01/22/1612:56 01/25/1613:48 1 <br />Arsenic <br />ND <br />1.0 <br />0.085 mg/Kg <br />01/22/16 12 56 01/25/16 13:48 1 <br />Barium <br />ND <br />0.50 <br />0.071 mg/Kg <br />01/22/1612:56 01/25/1613:48 1 <br />TestAmerica Pleasanton <br />Page 14 of 27 1/28/2016 <br />U P_005969 <br />