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Etc Laboratories, Ir Analytical & Environmental Services As Client: Union Pacific R it Road Report Date: March 25, 1996 833 East 8th St eet Stockton, CA 95207 Received Date: March 14, 1996 Thursday 10:01/TGN Attn.: Jack Dishman (209) 942-5358 x FAX (209) 942-5276 Project Name: Project #: Purchase order #: Audit 177019 Normal Turnaround Certificate of Analysis Lab#: 9605463 Sample ID: Title 22 Characterization Matrix: Sludge Sampled By: Jack Dishma Date: 03/08/1996 Time: 14:30 Fish Bioassay ................ .......... 612 mg/L Antimony ..................... .......... ND mg/Kg 5 Arsenic ...................... .......... ND mg/Kg 5 Barium ....................... .......... 23.1 mg/K9 Beryllium .................... .......... ND mg/K9 Cadmium ...................... .......... ND mg/K9 Chromium, Total .............. .......... 5.09 mg/Kg 1 Copper ....................... .......... 30.9 mg/Kg 1 Cobalt ....................... .......... ND mg/K9 Molybdenum ................... .......... 4.86 mg/K9 Nickel ....................... .......... ND mg/K9 Zinc ......................... .......... 74.7 mg/K9 Mercury ...................... .......... ND mg/K9 Soluble Antimony on WET Extra t......... ND mg/L Soluble Arsenic on WET Extrac .......... ND mg/L Soluble Barium on WET Extract .......... 1.29 mg/L Soluble Beryllium on WET Extr ct........ ND mg/L Soluble Cadmium on WET Extrac .......... ND mg/L Soluble Chromium on WET Extra t......... 0.12 mg/L Soluble Copper on WET Extract .......... 0.33 mg/L Soluble Cobalt on WET Extract .......... ND mg/L Soluble Lead on WET Extract.. .......... 0.34 mg/L Soluble Molybdenum on WET Ext Iact ....... 0.21 mg/L Soluble Nickel on WET Extract. ND mg/L Soluble Silver on WET ExtractJI.......... I.......... ND mg/L Soluble Thallium on WET Extra t......... ND mg/L Soluble Zinc on WET Extract.. .......... 4.62 mg/L Soluble Mercury on WET Extrac .......... ND mg/L Flash Point (Closed Cup) ..... .......... >200 Degrees F pH........................... .......... 6.13 Units ed Sub -Contract 03/16/1996 96047732 EPA 6010 03/18/1996 96047578 EPA 6010 03/18/1996 96047578 0.7 EPA 6010 03/18/1996 96047578 0.7 EPA 6010 03/18/1996 96047578 0.7 EPA 6010 03/18/1996 96047578 .5 EPA 6010 03/18/1996 96047578 .5 EPA 6010 03/18/1996 96047578 2.5 EPA 6010 03/18/1996 96047578 2.5 EPA 6010 03/18/1996 96047578 2.5 EPA 6010 03/18/1996 96047578 1.5 EPA 6010 03/18/1996 96047578 0.07 EPA 7471 03/18/1996 96047543 0.2 EPA 6010 03/19/1996 96047577 0.2 EPA 6010 03/19/1996 96047577 0.1 EPA 6010 03/19/1996 96047577 0.1 EPA 6010 03/19/1996 96047577 0.1 EPA 6010 03/19/1996 96047577 0.1 EPA 6010 03/19/1996 96047577 0.1 EPA 6010 03/19/1996 96047577 0.1 EPA 6010 03/19/1996 96047577 0.2 EPA 6010 03/19/1996 96047577 0.1 EPA 6010 03/19/1996 96047577 0.1 EPA 6010 03/19/1996 96047577 0.1 EPA 6010 03/19/1996 96047577 0.3 EPA 6010 03/19/1996 96047577 0.1 EPA 6010 03/19/1996 96047577 0.004 EPA 7471 03/18/1996 96047550 EPA 1010M 03/21/1996 96047685 EPA 9045 03/14/1996 96047458 14859 East Clark Avenue, Industry, California 91745-1396 (818) 336-2139 FAX (818) 336-2634 14859 East Clark Avenue, Industry, California 91745-1396 (818) 336-2139 FAX (818) 336-2634