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Client United Pumping Service <br />Project/Site: UPRR-Filter Bin Stockt n <br />Client Sample ID: UPS13111 <br />Date Collected: 11/11(13 08:00 <br />Date Received: 11122/1316:30 <br />Method: 8260B - Volatile Organic C <br />Analyte <br />1,1, 2, 2 -Tetrachloroethane <br />Tetrachloroethene <br />Toluene <br />1,2,3-TricNorobenzene <br />1, 2, 4-Tn ch I o roben zone <br />1.1,1-Tnchloroethene <br />1,1.2-Tnehloroethens <br />Trichloroethene <br />Trichlorofluoromethane <br />1, 2, 3-Tnchlompropa ns <br />1.1,2-Tdchloro-t, 2.2-trifluoroethane <br />1,2,4-Trimethylbenzene <br />1, 3, 5-Trimethylbenzene <br />Vinyl acetate <br />Vinyl chloride <br />Xylenes, Total <br />2,2-Dichloropropane <br />Surrogate <br />4-Bromo6uorobenzene <br />1,2-Dkhkroethane-d4 (Surr) <br />Toluene -d8 (Surr) <br />Method: 8015B - Diesel Range <br />Analyte <br />Diesel Range Organics [C10 -C28] <br />Motor Oil Range Organics <br />[C24 -C36] <br />Sunogate <br />p-Terphenyl <br />Method: 60108 - Metals (ICP) <br />Ana" <br />Antimony <br />Arsenic <br />Barium <br />Beryllium <br />Cadmium <br />Chromium <br />Cobalt <br />Copper <br />Lead <br />Molybdenum <br />Nickel <br />Selenium <br />Silver <br />ThaBlum <br />Vanadium <br />Zinc <br />Client Sample Results <br />TestAmerica Job ID: 720-54010-1 <br />CA <br />Lab Sample ID: 720-54010-1 <br />Matrix: Solid <br />ornpounds(GC/MS)(Continued) <br />Result Qualifier <br />RL <br />MDL Unit <br />D Prepared <br />Analyzed <br />DIl Fac <br />ND <br />NO <br />500 <br />ug/Kg <br />11/25/1312:00 <br />11/25/1312:54 <br />100 <br />0.92 <br />NO <br />500 <br />ug/Kg <br />11/25/13 12:00 <br />11/25/13 12.54 <br />100 <br />mg/Kg <br />ND <br />500 <br />ug/Kg <br />11/2511312:00 <br />11/25/1312:54 <br />100 <br />11/2611317:29 <br />NO <br />500 <br />ug/Kg <br />11/25/1312:00 <br />11125/1312.54 <br />100 <br />1112711317:29 <br />NO <br />500 <br />ug/Kg <br />11125/1312:00 <br />11125/1312:54 <br />100 <br />1 <br />ND <br />Soo <br />ug/Kg <br />11/25/1312:00 <br />11/25/1312.54 <br />100 <br />41 <br />NO <br />500 <br />ug/Kg <br />11/25/1312:00 <br />11/25/1312:54 <br />100 <br />0.46 <br />NO <br />5D0 <br />ug/Kg <br />11/25/1312:00 <br />11/25/1312:54 <br />100 <br />mg/Kg <br />NO <br />5o0 <br />ugft <br />11/2511312:00 <br />11/25/1312:54 <br />100 <br />11/26/1317:29 <br />NO <br />500 <br />ug/Kg <br />11/25/1312:00 <br />11/2511312:54 <br />100 <br />11/27/1317:29 <br />NO <br />500 <br />ug/Kg <br />11/25/1312:00 <br />11125/1312:54 <br />100 <br />1 <br />760 <br />500 <br />ug/Kg <br />11/25/1312:00 <br />11/25/1312:54 <br />100 <br />NO <br />NO <br />500 <br />ug/Kg <br />11/25/1312:00 <br />11/2511312:54 <br />100 <br />14 <br />NO <br />5000 <br />ug/Kg <br />11/25/1312:00 <br />11/2511312:54 <br />100 <br />NO <br />500 <br />ug/Kg <br />11125/1312:00 <br />11/2511312:54 <br />100 <br />NO <br />1000 <br />ug/Kg <br />11/25/131200 <br />11/2511312:54 <br />100 <br />ND <br />500 <br />ug/Kg <br />11/2511312:00 <br />11/251131254 <br />100 <br />%Recovery Qualifier <br />Limits <br />Prepared <br />Analyzed <br />DB Fac <br />98 <br />66-148 <br />11/25x1312.•00 <br />1183113 1254 <br />100 <br />104 <br />62-137 <br />11/2513 1200 <br />1112313 12,54 <br />100 <br />97 <br />65.141 <br />11/25131200 <br />11/251312:54 <br />100 <br />nice (DRO) (GC) <br />Result Qualifier <br />RL <br />MDL Unit <br />D Prepared <br />Analyzed <br />Oil Fee <br />99000 <br />3000 <br />mg/Kg <br />11/25/13 20:58 <br />11/29/13 10.00 <br />5o <br />380000 <br />150000 <br />mg/Kg <br />11/25/13 20:58 <br />11/29/13 10:00 <br />50 <br />%Recovery Qualifier Limits Prepared Analyzed DO Fac <br />0 XD 31-114 11/2513 2058 11/29/13 10,-00 50 <br />Result Qualifier <br />RL <br />MDL Unit <br />D Prepared <br />Analyzed <br />DII Fac <br />ND <br />0.46 <br />MON; <br />11/26/1317:29 <br />11/2711317:29 <br />1 <br />NO <br />0.92 <br />mg/Kg <br />11/26/1317:29 <br />11127/1317:29 <br />1 <br />0.95 <br />0.46 <br />mg/Kg <br />11/2611317:29 <br />11/27/1317:29 <br />1 <br />NO <br />0.092 <br />mg/Kg <br />11/2611317:29 <br />11/27/1317:29 <br />1 <br />ND <br />0.11 <br />mg/Kg <br />11/26/1317:29 <br />1112711317:29 <br />1 <br />1.8 <br />0.46 <br />mg/Kg <br />1112611317:29 <br />11/27/1317:29 <br />1 <br />NO <br />0.18 <br />mg/Kc <br />11/2611317:29 <br />11/27/1317,29 <br />1 <br />41 <br />1.4 <br />mgMg <br />11/26/1317:29 <br />11/27/1317:29 <br />1 <br />41 <br />0.46 <br />mg/Kg <br />1112611317:29 <br />1112711317:29 <br />1 <br />34 <br />0.45 <br />mg/Kg <br />11/26/1317:29 <br />11/27/1317:29 <br />1 <br />0.68 <br />0.46 <br />mg/Kg <br />11/26/1317:29 <br />11/27/1317:29 <br />1 <br />ND <br />0.92 <br />mg/Kg <br />11/26/1317:29 <br />11/27/1317:29 <br />1 <br />ND <br />0.23 <br />mg/Kg <br />11/26/1317.29 <br />11/27/1317:29 <br />1 <br />ND <br />0.46 <br />mg/Kg <br />11/26/1317:29 <br />11/27/1317:29 <br />1 <br />NO <br />0.46 <br />mg/Kg <br />11/26/1317:29 <br />11/27/1317:29 <br />1 <br />10 <br />14 <br />mg/Kg <br />1112611317.29 <br />11/27/1317:29 <br />1 <br />TestAmerica Pleasanton <br />Page 7 of 31 12/2/2013 <br />U P_006007 <br />