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QC Sample Results <br />Client: United Pumping Service <br />Project/Site: UPRR-Filter Bin Stockt n, CA <br />Method: 8260B - Volatile Org nic Compounds (GC/MS) (Continued) <br />Lab Sample ID: MB 720-148916/5 <br />Matrix: Solid <br />Analysis Batch: 148916 <br />Analyte <br />1 1.1.2-Tetrachloro thsne <br />1. 1. 2,2 -Tetrachloroethane <br />Tetrachloroethane <br />Toluene <br />1.2,3-Tnchlorobenzene <br />1, 2,4-Trichlorobenzene <br />1,1,1-T6chloroethane <br />1,1,2 -Trichloroethane <br />Trichloroethene <br />Tnchloro0uoromethane <br />1,2, 3-Trichloropropa ne <br />1,1, 2-Tnchloro-1, 2,2-tri8 uoroathane <br />1, 2,4-Trimethylbenzene <br />1, 3, 5-Trlmeth ylbenzene <br />Vinyl acetate <br />Vinyl chloride <br />Xylenes, Total <br />2,2-Oichloropropane <br />Surrogate <br />4-Bromotluorobenzene <br />1 2-Dich/orcethane-d4 (Surr) <br />Toluene -d8 (Surr) <br />Lab Sample ID: LCS 720-148916/6 <br />Matrix: Solid <br />Analysis Batch: 148916 <br />Analyte <br />Methyl tert-butyl other <br />Acetone <br />Benzene <br />Dichlorobromomethane <br />Bromobenzene <br />Chlorobromomethane <br />Bromotonn <br />Bromomethane <br />2-Butanons (MEK) <br />n-Butylbenzene <br />sec-Butylbenzene <br />tert-Butylbenzene <br />Carbon disulfide <br />Carbon tetrachlonde <br />Chlorobenzene <br />Chloroethane <br />Chloroform <br />Chloromethane <br />2-Chlarotoluene <br />TestAmerica Job ID: 720-54010-1 <br />Client Sample ID: Method Blank <br />Prep Type: Total/NA <br />MB MB <br />LCS LCS <br />%Rec. <br />Result OualiRer <br />RL <br />MDL Unit <br />D Prepared Anal <br />Oil Fac <br />NO <br />500 <br />ug/Kg <br />11/25/13 09-32 <br />100 <br />ND <br />500 <br />ug/Kg <br />11/25/13 0932 <br />100 <br />ND <br />500 <br />ug/Kg <br />11/25/13 09 32 <br />100 <br />ND <br />500 <br />ug/Kg <br />11/25/13 09 32 <br />100 <br />ND <br />500 <br />ug/Kg <br />11/25/13 09 32 <br />100 <br />ND <br />500 <br />ug/Kg <br />11/25/13 09.32 <br />100 <br />ND <br />500 <br />ug/Kg <br />11/25/13 0932 <br />100 <br />ND <br />500 <br />ug/Kg <br />11/25/13 09 32 <br />100 <br />ND <br />500 <br />ug/Kg <br />11/25/13 09.32 <br />100 <br />ND <br />500 <br />ug/Kg <br />11/25/13 09 32 <br />100 <br />ND <br />500 <br />ug/Kg <br />11/25/13 09 32 <br />100 <br />ND <br />500 <br />ug/Kg <br />11/25/13 09 32 <br />100 <br />ND <br />500 <br />ug/Kg <br />11/25113 09 32 <br />100 <br />ND <br />500 <br />ug/Kg <br />11/25113 09 32 <br />100 <br />ND <br />5000 <br />ug/Kg <br />11/25/13 09.32 <br />100 <br />ND <br />500 <br />ug/Kg <br />11/25/13 0932 <br />100 <br />ND <br />1000 <br />ug/Kg <br />11/25/13 0932 <br />100 <br />ND <br />500 <br />ug/Kg <br />11/25/13 09.32 <br />100 <br />MB MB <br />6120 <br />ug/Kg <br />122 <br />66-143 <br />%Recovery Qualifier <br />Limits <br />Prepared Analyzed <br />Dil Fat <br />97 <br />66- 148 <br />112513 09 32 <br />100 <br />102 <br />62- 137 <br />1125113 09 32 <br />100 <br />95 <br />65-141 <br />1125113 09 32 <br />100 <br />Client Sample ID: Lab Control Sample <br />Prep Type: Total/NA <br />Spike <br />LCS LCS <br />%Rec. <br />Added <br />Result Qualifier <br />Unit <br />D % Rec <br />Limits <br />5000 <br />5450 <br />ug/Kg <br />109 <br />71-146 <br />25000 <br />25300 <br />ug/Kg <br />101 <br />12-234 <br />5000 <br />5300 <br />ug/Kg <br />106 <br />76-122 <br />5000 <br />5960 <br />ug/Kg <br />119 <br />BO -131 <br />5000 <br />5990 <br />ug/Kg <br />120 <br />77-125 <br />5000 <br />5510 <br />ug/Kg <br />110 <br />74-134 <br />5000 <br />6070 <br />ug/Kg <br />121 <br />54-149 <br />5000 <br />4930 <br />ug/Kg <br />99 <br />14-175 <br />25000 <br />25900 <br />ug/Kg <br />103 <br />58-159 <br />5000 <br />5920 <br />ug/Kg <br />118 <br />57-164 <br />5000 <br />5680 <br />ug/Kg <br />114 <br />62-153 <br />5000 <br />6040 <br />ug/Kg <br />121 <br />72-136 <br />5000 <br />5090 <br />ug/Kg <br />102 <br />13-151 <br />5000 <br />6190 <br />ug/Kg <br />124 <br />72-136 <br />5000 <br />5750 <br />ug/Kg <br />115 <br />81-128 <br />5000 <br />4930 <br />ug/Kg <br />99 <br />53-124 <br />5000 <br />5700 <br />ug/Kg <br />114 <br />75-133 <br />5000 <br />4660 <br />ug/Kg <br />93 <br />43-146 <br />5000 <br />6120 <br />ug/Kg <br />122 <br />66-143 <br />Page 13 of 31 <br />TestAmerica Pleasanton <br />12/2/2013 <br />UP_006013 <br />