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Pace Analytical Services,LLC <br /> 315 Chestnut Street <br /> aceAnalytical Virginia,MN 55792 <br /> www.pacelabs.com <br /> (218)742-1042 <br /> I <br /> QUALITY CONTROL DATA <br /> Project: UPRES/Stockton REV <br /> Pace Project No.: 1298347 <br /> MATRIX SPIKE&MATRIX SPIKE DILIF LICATE: 509055 509056 <br /> MS MSD <br /> 1297262001 Spike Spike MS MSD MS MSD %Rec Max <br /> Parameter Uni s Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qual <br /> Antimony mg/.:g 45.5 47.6 48.5 68.6 71.0 49 53 75-125 3 20 M1 <br /> Arsenic mg/ g 107 47.6 48.5 154 155 99 98 75-125 0 20 <br /> Barium mg/ g 223 47.6 48.5 269 274 97 105 75-125 2 20 <br /> Beryllium mg/ g 153 47.6 48.5 194 195 86 86 75-125 0 20 <br /> Cadmium mg/ g 88.4 47.6 48.5 137 138 102 103 75-125 1 20 <br /> Chromium mg/ g 108 47.6 48.5 153 155 94 97 75-125 1 20 <br /> Cobalt mg/ g 122 47.6 48.5 165 168 89 95 75-125 2 20 <br /> Copper mg/ g 164 47.6 48.5 201 199 78 73 75-125 1 20 M1 <br /> Lead mg/ g 85.0 47.6 48.5 126 126 86 84 75-125 0 20 <br /> Molybdenum mg/ 51.5 47.6 48.5 100 102 102 103 75-125 2 20 <br /> Nickel mg/ 50.2 47.6 48.5 95.1 96.8 94 96 75-125 2 20 <br /> Selenium mg/k g 95.7 47.6 48.5 147 146 107 104 75-125 0 20 <br /> Silver mg/k g 42.1 23.8 24.3 62.0 60.7 83 77 75-125 2 20 <br /> Thallium mg/k g 55.3 47.6 48.5 97.8 97.7 89 87 75-125 0 20 <br /> Vanadium mg/k g 133 47.6 48.5 183 181 105 98 75-125 1 20 <br /> Zinc mg/k 4 153 47.6 48.5 199 200 95 97 75-125 1 20 <br /> VEL® <br /> to <br /> JAN 18 2018 <br /> ENVIRONMEWAL HEALTH <br /> CE��,;�_`--- <br /> - "-INT <br /> Results presented on this paE a are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. <br /> REPORT OF LABORATORY ANALYSIS <br /> This report shall not be reproduced,except in full, <br /> Date: 10/30/2017 11:12 AM without the written consent of Pace Analytical Services,LLC. Page 7 of 26 <br />