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Client Sample Results <br />Client United Pumping Service <br />Result Qualifier <br />RL <br />MDL Unit <br />TestAmerica Job ID: 720-54166-1 <br />Analyzed <br />Project/Site: UPRR-Stockton Debris <br />in CA <br />16000 <br />250 <br />mg/Kg <br />12/07/13 10 04 <br />12/10/13 00:38 <br />100 <br />Client Sample ID: UPS131202 <br />OILY SAND <br />12000 <br />mg/Kg <br />Lab Sample ID: 720-54166-1 <br />12/10/13 00:38 <br />Date Collected: 12/02/13 11:45 <br />[C24 -C36] <br />Matrix: <br />Solid <br />Date Received: 12/04!1318:15 <br />%Recovery Qua/mer <br />Limits <br />Prepared <br />Analyzed <br />D8 Fac <br />Method: 8260B - Volatile Organic <br />ompounds (GC/MS) (Continued) <br />0 X D <br />40.130 <br />12017/13 10.04 <br />12110/13 0038 <br />Analyte <br />Result Qualifler <br />RL <br />MDL Unit <br />D Prepared <br />Analyzed <br />DII Fac <br />1,1,2.2 -Tetrachloroethane <br />NO <br />430 <br />ug/Kg <br />12110/1311:00 <br />12/1011318:04 <br />100 <br />Analyzed <br />Tetrachloroethane <br />ND <br />430 <br />ug/Kg <br />12/10/1311:00 <br />12/1011316:04 <br />100 <br />12/09/1318.23 <br />Toluene <br />NO <br />430 <br />ug/Kg <br />12110/13 11:00 <br />12!1011316:04 <br />100 <br />12/09/1318:23 <br />1,2,3-Trichlorohenzens <br />NO <br />430 <br />ug/Kg <br />12/10/1311:00 <br />12/10/1316:04 <br />100 <br />12/09/131823 <br />1,2,4-Trichlorobonzene <br />NO <br />430 <br />ug/Kg <br />12/10/1311:00 <br />12/1011316:04 <br />100 <br />12/09/131623 <br />1,1,1 -Trichloroethane <br />NO <br />430 <br />ug/Kg <br />12110/1311:00 <br />12/1011318:04 <br />100 <br />12/09/1318.23 <br />1,1,2 -Trichloroethane <br />ND <br />430 <br />ug/Kg <br />12/10/13 11:00 <br />12/10/13 16:04 <br />100 <br />12109/131823 <br />Trichloroethene <br />NO <br />430 <br />ug/Kg <br />12/10/13 11:00 <br />12/10/13 16:04 <br />100 <br />12109/1318.23 <br />Trichlorofluoromethane <br />NO <br />430 <br />ug/Kg <br />12/10/1311:00 <br />12/10/1316:04 <br />100 <br />12/09/1318,23 <br />1,2,3-Thchloropropene <br />NO <br />430 <br />ug/Kg <br />12/10/1311:00 <br />12110/1316:04 <br />100 <br />12/09/1316:23 <br />1,1,2-Trichloro-1,2,2-trtfluoroethane <br />NO <br />430 <br />ug1Kg <br />12/10/1311:00 <br />12110/1316:04 <br />100 <br />12/09/1318.23 <br />1,2,4-Trimethylbenzene <br />NO <br />430 <br />ug1Kg <br />12/10/1311:00 <br />12/1011316:04 <br />100 <br />12/09/1316:23 <br />1,3,5-Trimethylbenzene <br />ND <br />430 <br />uWKg <br />12/10/1311:00 <br />12/10/131604 <br />100 <br />12/09/1318:23 <br />Vinyl acetate <br />NO <br />4300 <br />ug/Kg <br />12/10/13 11:00 <br />12/10/13 16:04 <br />100 <br />12/09/1318:23 <br />Vinyl chloride <br />NO <br />430 <br />ug/Kg <br />12/10/13 11:00 <br />12/10/13 16:04 <br />100 <br />12/09/13 16 23 <br />Xylenes, Total <br />ND <br />870 <br />ug/Kg <br />12/10/1311:00 <br />12/10113 16,04 <br />100 <br />12109/13 18 23 <br />2,2-Dichloropropane <br />ND <br />430 <br />ug/Kg <br />12110/1311:00 <br />12/10/1316: D4 <br />100 <br />12109/1318:23 <br />Surrogate <br />%Recovery Qualifier <br />Limits <br />Prepared <br />Analyzed <br />D8 Fac <br />4-Bromofluorobenzene <br />106 <br />66-148 <br />12110113 11:00 <br />12/10/13 1604 <br />100 <br />1, 2-Drch/oroethane-d4 (Surr) <br />101 <br />62-137 <br />12/10/13 11:00 <br />12110113 16 04 <br />100 <br />Toluene -d8 (Surf) <br />101 <br />65-141 <br />12/10/13 11:00 <br />12110/13 1604 <br />100 <br />Method: 8015B - Diesel Range Organics (DRO) (GC) <br />Analyte <br />Result Qualifier <br />RL <br />MDL Unit <br />D Prepared <br />Analyzed <br />oil Fac <br />Diesel Range Organics [C10 -C28] <br />16000 <br />250 <br />mg/Kg <br />12/07/13 10 04 <br />12/10/13 00:38 <br />100 <br />Motor Oil Range Organics <br />44000 <br />12000 <br />mg/Kg <br />12/07/13 10.04 <br />12/10/13 00:38 <br />100 <br />[C24 -C36] <br />Surrogate <br />%Recovery Qua/mer <br />Limits <br />Prepared <br />Analyzed <br />D8 Fac <br />p-Terphenyl <br />0 X D <br />40.130 <br />12017/13 10.04 <br />12110/13 0038 <br />100 <br />Method: 6010B - Metals (ICP) <br />Analyte <br />Result Qualifier <br />RL <br />MDL Unit <br />D Prepared <br />Analyzed <br />Dil Fac <br />Antimony <br />NO <br />1.9 <br />mg/Kg <br />12/06/1316:57 <br />12/09/1318.23 <br />4 <br />Arsenic <br />5.8 <br />3.8 <br />mg/Kg <br />12/0611316:57 <br />12/09/1318:23 <br />4 <br />Barium <br />51 <br />1.9 <br />mg/Kg <br />12/05/1316:57 <br />12/09/131823 <br />4 <br />Beryllium <br />ND <br />0.38 <br />mg/Kg <br />12/06!131637 <br />12/09/131623 <br />4 <br />Cadmium <br />NO <br />0.48 <br />mg/Kg <br />12/06!1316:57 <br />12/09/1318.23 <br />4 <br />Chromium <br />11 <br />1.9 <br />mg/Kg <br />12/06/1316:57 <br />12109/131823 <br />4 <br />Cobalt <br />3.2 <br />0.76 <br />mg/Kg <br />12/08/1316.57 <br />12109/1318.23 <br />4 <br />Copper <br />39 <br />5.7 <br />mg/Kg <br />12/0611316:57 <br />12/09/1318,23 <br />4 <br />Lead <br />22 <br />1.9 <br />mg/Kg <br />12/06/1316:57 <br />12/09/1316:23 <br />4 <br />Molybdenum <br />7.2 <br />1.9 <br />mg/Kg <br />12/0611316:57 <br />12/09/1318.23 <br />4 <br />Nickel <br />8.1 <br />1.9 <br />mglKg <br />12/0611316:57 <br />12/09/1316:23 <br />4 <br />Selenium <br />ND <br />3.8 <br />mg/Kg <br />12/06/1316:57 <br />12/09/1318:23 <br />4 <br />Silver <br />ND <br />0.95 <br />mg/Kg <br />12/0611316:57 <br />12/09/1318:23 <br />4 <br />Thallium <br />ND <br />1.9 <br />mg/Kg <br />12/06/13 16:57 <br />12/09/13 16 23 <br />4 <br />Vanadium <br />19 <br />19 <br />mg/Kg <br />12106/1316:57 <br />12109/13 18 23 <br />4 <br />Zinc <br />81 <br />5.7 <br />mg/Kg <br />12/06/1316:57 <br />12109/1318:23 <br />4 <br />TestAmerica Pleasanton <br />Page 7 of 27 12/12/2013 <br />UP_006038 <br />