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QC Sample Results <br />Client: United Pumping Service ITestAmerica <br />Job ID'. 720-54166-1 <br />Project/Site: UPRR-Stockton Debris bin CA <br />Method: 8260B - Volatile Orgnic Compounds <br />(GC/MS) (Continued) <br />Lab Sample ID: LCS 720.149743/9 <br />Client Sample <br />ID: Lab Control Sample <br />Matrix: Solid <br />Prep Type: Total/NA <br />Analysis Batch: 149743 <br />Spike <br />LCS LCS <br />%Rec. <br />Ana" <br />Added <br />Result Qualliier <br />Unit <br />D %Ree <br />Limits <br />2,2-Dlchloropropene <br />5000 <br />5260 <br />ugiKg <br />105 <br />67-146 <br />LCS LCS <br />surroyere Recovery Qualifier <br />L1m11s <br />4-BromoRuoroberizene 100 <br />66.148 <br />1.2-Dichloroethane-d4 (Sun) 96 <br />62-137 <br />Toluene -d8 (Surr) 102 <br />65.141 <br />Lab Sample ID: LCSD 720-149743/ 0 <br />Client <br />Sample ID: Lab Control <br />Sample Dup <br />Matrix: Solid <br />Prep Type: Total/NA <br />Analysis Batch: 149743 <br />Spike <br />LCSD LCSD <br />%Rec. <br />RPD <br />Anslyte <br />Added <br />Result Qualifier <br />Unit <br />D %Rec <br />Limits <br />RPD <br />Limit <br />Methyl tart -butyl ethA <br />5000 <br />4860 <br />ug/Kg <br />97 <br />71.146 <br />10 <br />20 <br />Acetone <br />25000 <br />20300 <br />ug/Kg <br />81 <br />12-234 <br />18 <br />30 <br />Benzene <br />5000 <br />5200 <br />ug/Kg <br />104 <br />76-122 <br />0 <br />20 <br />Dichlorebromomethane <br />5000 <br />4730 <br />ug/Kg <br />95 <br />80-131 <br />4 <br />20 <br />Bromobenzene <br />5000 <br />5110 <br />ug/Kg <br />102 <br />77-125 <br />0 <br />20 <br />Chlorobromomethane <br />5000 <br />4880 <br />ug/Kg <br />98 <br />74-134 <br />5 <br />20 <br />Bromororm <br />5000 <br />4760 <br />ug/Kg <br />95 <br />54-149 <br />7 <br />20 <br />Bromomethane <br />5000 <br />3830 <br />ug/Kg <br />77 <br />14-175 <br />5 <br />20 <br />2-Butanone (MEK) <br />25000 <br />21700 <br />ug/Kg <br />87 <br />58-159 <br />13 <br />20 <br />n-Butylbenzene <br />5000 <br />5900 <br />ug/Kg <br />118 <br />57.164 <br />2 <br />20 <br />sec -Bu tylbenzene <br />5000 <br />5530 <br />ug./Kg <br />111 <br />62-153 <br />3 <br />20 <br />tert-Butylbenzene <br />5000 <br />5510 <br />ug/Kg <br />110 <br />72-136 <br />2 <br />20 <br />Carbon disulfide <br />5000 <br />4760 <br />ug/Kg <br />95 <br />13- 151 <br />1 <br />20 <br />Carbon teirachlonde <br />5000 <br />5210 <br />ug/Kg <br />104 <br />72-136 <br />1 <br />20 <br />Chlorobenzene <br />5000 <br />5260 <br />ug/Kg <br />105 <br />81-128 <br />0 <br />20 <br />Chloroethane <br />5000 <br />4010 <br />ug/Kg <br />80 <br />53-124 <br />2 <br />20 <br />Chloroform <br />5000 <br />5040 <br />ug/Kg <br />101 <br />75.133 <br />1 <br />20 <br />Chlorcmethane <br />5000 <br />4100 <br />ugiKg <br />82 <br />43-146 <br />1 <br />20 <br />2-Chlarotoluene <br />5000 <br />5590 <br />ug/Kg <br />112 <br />66-143 <br />3 <br />20 <br />4-Chiarotoluene <br />5000 <br />5400 <br />ug/Kg <br />108 <br />73-136 <br />2 <br />20 <br />Chlorodibromomethane <br />5000 <br />4720 <br />ug/Kg <br />94 <br />76-134 <br />5 <br />20 <br />1,2 -Dichlorobenzene <br />5000 <br />5240 <br />ug/Kg <br />105 <br />77.140 <br />0 <br />20 <br />1,3 -Dichlorobenzene <br />5000 <br />5400 <br />ug/Kg <br />108 <br />71-135 <br />2 <br />20 <br />1,4 -Dichlorobenzene <br />5000 <br />5340 <br />ug/Kg <br />107 <br />76-130 <br />1 <br />20 <br />1,3-Dichloropropane <br />5000 <br />4840 <br />ug/Kg <br />97 <br />73-133 <br />5 <br />20 <br />1.1-Dichloropropens <br />5000 <br />5700 <br />ug/Kg <br />114 <br />61 -134 <br />1 <br />20 <br />1,2-Dibromo-3-Chloropropane <br />5000 <br />4730 <br />ug/Kg <br />95 <br />52-156 <br />9 <br />20 <br />Ethylene Dibromide <br />5000 <br />4880 <br />ug/Kg <br />98 <br />80-138 <br />8 <br />20 <br />Dibromomethane <br />5000 <br />5080 <br />ug/Kg <br />102 <br />76-139 <br />6 <br />20 <br />Dichlorodifluoromethane <br />5000 <br />3960 <br />ug/Kg <br />79 <br />30.120 <br />1 <br />20 <br />1,1-Dichloroethane <br />5000 <br />5160 <br />ugiKg <br />103 <br />79-125 <br />0 <br />20 <br />1.2-Dichloroethane <br />5000 <br />4560 <br />ug/Kg <br />94 <br />67.126 <br />4 <br />20 <br />1,1-Dichloroethene <br />5000 <br />4980 <br />ug/Kg <br />100 <br />74.122 <br />0 <br />20 <br />cis- 1,2-Dichloroethene <br />5000 <br />5090 <br />ug/Kg <br />102 <br />77-132 <br />1 <br />20 <br />trans-1,2-Dichloroethene <br />5000 <br />5340 <br />ugiKg <br />107 <br />74- 128 <br />0 <br />20 <br />1.2-Dichloropropane <br />5000 <br />5000 <br />ug(Kg <br />100 <br />84-129 <br />2 <br />20 <br />TestAmerica Pleasanton <br />Page 12 of 27 12/12/2013 <br />U P_006043 <br />