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Client: Union Pacific Railroac <br />Project/Site: UPRR-Stockton <br />Method: 82606/CA LU <br />Lab Sample ID: 720-69606 <br />Matrix: Solid <br />Analysis Batch: 195268 <br />Analyte <br />Benzene <br />Ethylbenzene <br />Toluene <br />m -Xylene & p -Xylene <br />o -Xylene <br />Surrogate <br />4-Bromofluorobenzene <br />1,2-Dichloroethene-& (Sun) <br />Toluene -d8 (Sun) <br />Lab Sample ID: 720-696 <br />Matrix: Solid <br />Analysis Batch: 195268 <br />Analyte <br />Benzene <br />Ethylbenzene <br />Toluene <br />m -Xylene 8 p -Xylene <br />o -Xylene <br />QC Sample Results <br />- 8260B / CA LUFT MS (Continued) <br />1 MS <br />Sample Sample <br />Spike <br />Result Qualifier <br />Added <br />NO <br />48.8 <br />NO <br />48.8 <br />NO <br />48.8 <br />NO <br />48.8 <br />NO <br />48.8 <br />MS MS <br />70-130 <br />%Recovery Qualifier <br />Limits <br />81 <br />45-131 <br />102 <br />60-140 <br />79 <br />58-140 <br />Surrogate <br />4-Brvmoftuorobenzene <br />1,2-Dichloroethene-d4 (Sun) <br />Toluene -d8 (sun) <br />Method: 8015B - Diesel <br />Lab Sample ID: MB 720-195 <br />Matrix: Solid <br />Analysis Batch: 195283 <br />Analyte <br />Diesel Range Organics [C10 -C28] <br />Motor Oil Range Organics [C24 -C36] <br />Surrogate <br />p-Terphenyl <br />Lab Sample ID: LCS 720-19E <br />Matrix: Solid <br />Analysis Batch: 195283 <br />Analyte <br />Diesel Range Organics <br />[C10 -C28] <br />MSD <br />Sample Sample <br />Spike <br />Result Qualifier <br />Added <br />NO <br />49.3 <br />ND <br />49.3 <br />ND <br />49.3 <br />NO <br />49.3 <br />NO <br />49.3 <br />MSD MSD <br />70-130 <br />;Recovery Qualer <br />Limits <br />83 <br />45-131 <br />110 <br />60-140 <br />74 <br />58-140 <br />range Organics (DRO) (GC) <br />29/1-A <br />4 <br />M8 MB <br />Prep Type: Total/NA <br />Result Qualifier <br />RL <br />ND <br />1.0 <br />ND <br />50 <br />MB MB <br />ug/Kg <br />%Recovery Qualifier <br />Limits <br />101 <br />40-130 <br />Spike <br />Added <br />83.3 <br />MS MS <br />Prep Type: Total/NA <br />Result Qualifier <br />Unit <br />48.9 <br />ug/Kg <br />41.8 <br />ug/Kg <br />53.0 <br />ug/Kg <br />39.8 <br />ug/Kg <br />36.1 <br />ug/Kg <br />MSD MSD <br />Prep Type: Total/NA <br />Result Qualifier <br />Unit <br />47.1 <br />ug/Kg <br />41.6 <br />ug/Kg <br />51.1 <br />ug/Kg <br />39.1 <br />ug/Kg <br />34.9 <br />ug/Kg <br />MDL Unit <br />mg/Kg <br />mg/Kg <br />TestAmerica Job ID: 720-69606-1 <br />Client Sample ID: BIN MR 605 PL <br />Client Sample ID: BIN MR 605 PL <br />Prep Type: Total/NA <br />Prep Batch: 195274 <br />Prep Type: Total/NA <br />Prep Batch: 195274 <br />D %Rec <br />%Rec. <br />D %Rec <br />Limits <br />10D <br />70-130 <br />86 <br />65-130 <br />109 <br />70-130 <br />82 <br />70-130 <br />74 <br />68-130 <br />Client Sample ID: BIN MR 605 PL <br />Prep Type: Total/NA <br />Prep Batch: 195274 <br />Client Sample ID: Method Blank <br />Prep Type: Total/NA <br />Prep Batch: 195329 <br />D Prepared Analyzed DII Fac <br />01108/1614:42 01/0811618:07 1 <br />01108/1614:42 01/08/1618:07 1 <br />Prepared Analyzed Oil Fac <br />01106116 14.42 011DB116 18 07 1 <br />Client Sample ID: Lab Control Sample <br />Prep Type: Total/NA <br />Prep Batch: 195329 <br />LCS LCS %Rec. <br />Result Qualifier Unit D %Rec Limits <br />95.8 mgfKg 115 50-150 <br />Page 8 of 23 <br />TestAmerica Pleasanton <br />1/19/2016 <br />U P_006066 <br />%Rec. <br />RPD <br />D %Rec <br />Limits <br />RPD <br />Limit <br />96 <br />70-130 <br />4 <br />20 <br />84 <br />65-130 <br />1 <br />20 <br />104 <br />70-130 <br />4 <br />20 <br />79 <br />70-130 <br />2 <br />20 <br />71 <br />68-130 <br />4 <br />20 <br />Client Sample ID: Method Blank <br />Prep Type: Total/NA <br />Prep Batch: 195329 <br />D Prepared Analyzed DII Fac <br />01108/1614:42 01/0811618:07 1 <br />01108/1614:42 01/08/1618:07 1 <br />Prepared Analyzed Oil Fac <br />01106116 14.42 011DB116 18 07 1 <br />Client Sample ID: Lab Control Sample <br />Prep Type: Total/NA <br />Prep Batch: 195329 <br />LCS LCS %Rec. <br />Result Qualifier Unit D %Rec Limits <br />95.8 mgfKg 115 50-150 <br />Page 8 of 23 <br />TestAmerica Pleasanton <br />1/19/2016 <br />U P_006066 <br />