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Client: United Pumping Service <br />Project/Site: UPRR-Stockton <br />Method: 601013- Metals (IC ) (Continued) <br />Lab Sample ID: 440 -2133 -A -1-I RISD ^5 <br />Matrix: Solid <br />Analysis Batch: 8680 <br />Analyte <br />Barium <br />Beryllium <br />Cadmium <br />Chromium <br />Cobalt <br />Copper <br />Lead <br />Molybdenum <br />Nickel <br />Selenium <br />Thallium <br />Zinc <br />Silver <br />Lab Sample ID: 440 -2133 -A -1-I <br />Matrix: Solid <br />Analysis Batch: 9608 <br />Analyte <br />Selenium <br />Lab Sample ID: 440 -2133 -A -1-K I <br />Matrix: Solid <br />Analysis Batch: 8680 <br />Analyte <br />Antimony - <br />Arsenic <br />Barium <br />Beryllium <br />Cadmium <br />Chromium <br />Cobalt <br />Copper <br />Lead <br />Molybdenum <br />Nickel <br />Selenium <br />Thallium <br />Zinc <br />Silver <br />Lab Sample ID: 440 -2133 -A -1-K I <br />Matrix: Solid <br />Analysis Batch: 9608 <br />Analyte <br />Selenium <br />Sample Sample <br />Result Qualifier <br />330 <br />ND <br />2.2 <br />31 <br />1.5 <br />110 <br />4.1 <br />4.7 <br />13 <br />9.0 <br />ND <br />180 <br />ND <br />SD ^5 <br />Sample Sample <br />Result Qualifier <br />6.5 <br />^5 <br />Sample Sample <br />Result Qualifier <br />ND <br />2.1 <br />330 <br />ND <br />2.2 <br />31 <br />1.5 <br />110 <br />4.1 <br />4.7 <br />13 <br />9.0 <br />ND <br />180 <br />ND <br />^5 <br />Sample Sample <br />Result Qualifier <br />6.5 <br />QC Sample Results <br />Spike <br />Added <br />51.0 <br />51.0 <br />51.0 <br />51.0 <br />51.0 <br />51.0 <br />51.0 <br />51.0 <br />51.0 <br />51.0 <br />51.0 <br />51.0 <br />25.5 <br />TestAmerica Job ID: 440-2207-2 <br />Client Sample ID: Matrix Spike Duplicate <br />Prep Type: Total/NA <br />Prep Batch: 6998 <br />Spike <br />MSD MSD <br />Client Sample ID: Matrix Spike Duplicate <br />%Rec. RPD <br />Prep Type: Total/NA <br />Result Qualifier <br />Unit <br />Prep Batch: 6998 <br />MSD MSD <br />51.0 <br />%Rec. RPD <br />Result Qualifier <br />Unit <br />D %Rec Limits RPD Limit <br />402 <br />mg/Kg <br />48.2 <br />mg/Kg <br />47.8 <br />mg/Kg <br />Prep Type: Total/NA <br />81.1 <br />mg/Kg <br />47.3 <br />mg/Kg <br />MS MS <br />169 <br />mg/Kg <br />%Rec. <br />50.9 <br />mg/Kg <br />Unit <br />49.1 <br />mg/Kg <br />49.0 <br />59.7 <br />mg/Kg <br />78 <br />53.9 <br />mg/Kg <br />43.4 <br />44.8 <br />mg/Kg <br />75-125 <br />234 <br />mg/Kg <br />mg/Kg <br />24.2 <br />mg/Kg <br />49.0 <br />Client Sample ID: Matrix Spike Duplicate <br />Prep Type: Total/NA <br />Prep Batch: 6998 <br />Spike <br />MSD MSD <br />%Rec. RPD <br />Added <br />Result Qualifier <br />Unit <br />D %Rec <br />Limits RPD Limit <br />51.0 <br />48.8 <br />mg/Kg <br />83 <br />75-125 4 20 <br />Client <br />Sample ID: Matrix Spike <br />Prep Type: Total/NA <br />Prep Batch: 6998 <br />Spike <br />MS MS <br />%Rec. <br />Added <br />Result Qualifier <br />Unit <br />D %Rec <br />Limits <br />49.0 <br />39.7 <br />mg/Kg <br />78 <br />75-125 <br />49.0 <br />43.4 <br />mg/Kg <br />B4 <br />75-125 <br />49.0 <br />385 4 <br />mg/Kg <br />112 <br />75-125 <br />49.0 <br />45.1 <br />mg/Kg <br />92 <br />75-125 <br />49.0 <br />45.0 <br />mg/Kg <br />87 <br />75-125 <br />49.0 <br />77.4 <br />mg/Kg <br />95 <br />75-125 <br />49.0 <br />44.5 <br />mg/Kg <br />88 <br />75-125 <br />49.0 <br />163 <br />mg/Kg <br />103 <br />75-125 <br />49.0 <br />47.9 <br />mg/Kg <br />89 <br />75-125 <br />49.0 <br />46.4 <br />mg/Kg <br />85 <br />75-125 <br />49.0 <br />57.0 <br />mg/Kg <br />91 <br />75-125 <br />49.0 <br />50.1 <br />mg/Kg <br />84 <br />75-125 <br />49.0 <br />41.0 <br />mg/Kg <br />82 <br />75-125 <br />49.0 <br />228 <br />mg/Kg <br />97 <br />75-125 <br />24.5 <br />22.8 <br />mg/Kg <br />89 <br />75-125 <br />Client <br />Sample ID: Matrix Spike <br />Prep Type: Total/NA <br />Prep Batch: 6998 <br />Spike <br />MS MS <br />%Rec. <br />Added <br />Result Qualifier <br />Unit <br />D %Rec <br />Limits <br />49.0 <br />47.1 <br />mg/Kg <br />83 <br />75.125 <br />RECEIVENNAmerica Irvine <br />Page 10 of 20 FEB 18 2014 11/26/2013 <br />ENVIRONMENTAL <br />HEALTH DEPARTMENT <br />