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tiff eurofins Calsci Glossary of Terms and Qualifiers Page 6 of 10 Work Order: 17-10-0556 Page 1 of 1 Qualifiers 1 2 3 4 5 6 7 B BU BV Cl E ET HD HDH HDL J JA ME ND Q SG X Z Definition See applicable analysi comment. Less than the indicate value. Greater than the indic ed value. Surrogate compound r covery was out of control due to a required sample dilution. Therefore, the sample data was reported without further clarification. Surrogate compound r covery was out of control due to matrix interference. The associated method blank surrogate spike compound was in control and, therefor , the sample data was reported without further clarification. Recovery of the Matrix pike (MS) or Matrix Spike Duplicate (MSD) compound was out of control due to suspected matrix interference. The associated LCS recove was in control. The MS/MSD RPD wa out of control due to suspected matrix interference. The PDS/PDSD or PE /PESD associated with this batch of samples was out of control due to suspected matrix interference. Surrogate recovery bel w the acceptance limit. Surrogate recovery ab a the acceptance limit. Pe Analyte was present in he associated method blank. Sample analyzed after olding time expired. Sample received after olding time expired. O 2017 See case narrative. Concentration exceeds he calibration range. ENVIRONMENTAL HEALTH Sample was extracted ast end of recommended max. holding time. DEPARTMENT The chromatographic p ttern was inconsistent with the profile of the reference fuel standard. The sample chromatogr phic pattern for TPH matches the chromatographic pattern of the specified standard but heavier hydrocarbons were also present (or d tected). The sample chromatogr phic pattern for TPH matches the chromatographic pattern of the specified standard but lighter hydrocarbons were also present (or detecte ). Analyte was detected at a concentration below the reporting limit and above the laboratory method detection limit. Reported value is estimated. Analyte positively identi ed but quantitation is an estimate. LCS Recovery Percenta a is within Marginal Exceedance (ME) Control Limit range (+/- 4 SD from the mean). Parameter not detected t the indicated reporting limit. Spike recovery and RP control limits do not apply resulting from the parameter concentration in the sample exceeding the spike concentration by a facto of four or greater. The sample extract was ubjected to Silica Gel treatment prior to analysis. % Recovery and/or RPD out -of -range. Analyte presence was n t confirmed by second column or GC/MS analysis. Solid - Unless otherwise indicated, solid sample data is reported on a wet weight basis, not corrected for % moisture. All QC results are reported on a wet weight basis. Any parameter identified in 40CFR Part 136.3 Table II that is designated as "analyze immediately" with a holding time of — 15 minutes (40CFR-136.3 Table ll, f)otnote 4), is considered a "field" test and the reported results will be qualified as being received outside of the stated holding time unless received at the laboratory within 15 minutes of the collection time. A calculated total result (ample: Total Pesticides) is the summation of each component concentration and/or, if "J" flags are reported, estimated concentration. Component concentrations showing not detected (ND) are summed into the calculated total result as zero concentrations. 7440 Lincoln Woy, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 Page 22 of 26 N CE