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LABORATORY CONTROL SAMPLE EVALUATION REPORT <br />GC/MS Volatiles <br />Client Lot #....- G5C070225 <br />Work Order <br />#...: <br />G60M41AC-LCS <br />Matrix.........: SOLID <br />LCS Lot -Sample#: G5C240�000-445 <br />G60M41AD-LCSD <br />PERCENT <br />RECOVERY <br />RPD <br />PARAMETER <br />RECOVERY <br />LIMITS <br />RPA <br />LIMITS <br />METHOD <br />Trichloroethene <br />118 <br />(67 <br />- 135) <br />SW846 <br />8260B <br />106 <br />(67 <br />- 135) <br />10 <br />(0-38) <br />SW846 <br />8260E <br />1,2-Dichloropropane <br />118 <br />(74 <br />- 120) <br />SW846 <br />8260B <br />106 <br />(74 <br />- 120) <br />11 <br />(0-30) <br />SW846 <br />8260B <br />Dibromomethane <br />92 <br />(74 <br />- 120) <br />SW846 <br />8260B <br />82 <br />(74 <br />- 120) <br />11 <br />(0-150) <br />SW846 <br />8260E <br />Bromodichloromethane <br />96 <br />(73 <br />- 120) <br />SW846 <br />6260B <br />86 <br />(73 <br />- 120) <br />11 <br />(0-23) <br />SW846 <br />8260B <br />cis-1,3-Dichloropropene <br />108 <br />(74 <br />- 120) <br />SW846 <br />8260B <br />98 <br />(74 <br />- 120) <br />11 <br />(0-27) <br />SW846 <br />8260B <br />Toluene <br />111 <br />(79 <br />- 120) <br />SW846 <br />8260D <br />100 <br />(79 <br />- 120) <br />10 <br />(0-17) <br />SW846 <br />8260B <br />trans-1,3-Dichloroprope <br />a <br />92 <br />(72 <br />- 120) <br />SW846 <br />8260B <br />83 <br />(72 <br />- 120) <br />10 <br />(0-29) <br />SW846 <br />8260B <br />1,1,2 -Trichloroethane <br />96 <br />(75 <br />- 120) <br />SW846 <br />8260B <br />83 <br />(75 <br />- 120) <br />15 <br />(0-17) <br />SW846 <br />8260B <br />Tetrachloroethene <br />108 <br />(75 <br />- 121) <br />SW846 <br />8260B <br />93 <br />(75 <br />- 121) <br />14 <br />(0-21) <br />SW846 <br />8260B <br />1,3-Dichloropropane <br />103 <br />(77 <br />- 120) <br />SW846 <br />8260B <br />88 <br />(77 <br />- 120) <br />16 <br />(0-25) <br />SW846 <br />6260E <br />Dibromochloromethane <br />90 <br />(72 <br />- 120) <br />SW846 <br />8260B <br />78 <br />(72 <br />- 120) <br />14 <br />(0-27) <br />SW846 <br />8260B <br />1,2-Dibromoethane (EDB) <br />93 <br />(75 <br />- 120) <br />SW846 <br />8260B <br />82 <br />(75 <br />- 120) <br />13 <br />(0-26) <br />SW846 <br />8260B <br />Chlorobenzene <br />109 <br />(77 <br />- 120) <br />SW846 <br />8260E <br />96 <br />(77 <br />- 120) <br />12 <br />(0-17) <br />SW846 <br />8260B <br />1,1,1,2-Tetrachloroetha <br />7 <br />105 <br />92 <br />(76 <br />(76 <br />- 120) <br />- 120) <br />13 <br />(0-21) <br />SW846 <br />SW846 <br />8260B <br />8260E <br />Ethylbenzene <br />116 <br />(79 <br />- 120) <br />SW846 <br />8260B <br />103 <br />(79 <br />- 120) <br />12 <br />(0-20) <br />SW846 <br />8260B <br />m -Xylene & p -Xylene <br />114 <br />(80 <br />- 120) <br />SW846 <br />8260B <br />102 <br />(80 <br />- 120) <br />11 <br />(0-19) <br />SW846 <br />8260B <br />o -Xylene <br />118 <br />(78 <br />- 120) <br />SW846 <br />8260B <br />102 <br />(78 <br />- 120) <br />14 <br />(0-22) <br />SW846 <br />8260B <br />Styrene <br />118 <br />(69 <br />- 120) <br />SW846 <br />826013 <br />104 <br />(69 <br />- 120) <br />12 <br />(0-30) <br />SW846 <br />8260B <br />Bromoform <br />81 <br />(64 <br />- 120) <br />SW846 <br />8260B <br />68 <br />(64 <br />- 120) <br />16 <br />(0-22) <br />SW846 <br />8260B <br />Isopropylbenzene <br />112 <br />(78 <br />- 120) <br />SW846 <br />8260E <br />97 <br />(78 <br />- 120) <br />14 <br />(0-20) <br />SW846 <br />8260B <br />Bromobenzene <br />114 <br />(77 <br />- 120) <br />SW846 <br />8260B <br />103 <br />(77 <br />- 120) <br />9.8 <br />(0-21) <br />SW846 <br />8260B <br />(Continued on next page) <br />G5C070225 STL Sacramento (916) 373 - 5600 18 of 67 <br />