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UNION PACIFIC RAILROAD <br />Client Sample ID: 03072005 <br />Lot -Sample #...: GSC070$25-001 <br />Date Sampled...: 03/07/t5 <br />Prep Date......: 03/14/ 5 <br />Prep Batch #...: 507039 <br />Dilution Factor: 10000 <br />GC Semivolatiles <br />Work Order #.... G5PG41AE Matrix.......... SOLID <br />Date Received..: 03/07/05 <br />Analysis Date..: 03/23/05 <br />Method.........: SW846 8015 MOD <br />PARAMETER RESULT <br />TPH (as Diesel) ND <br />TPH (as Motor Oil) ND <br />Unknown hydrocarbon 290000 <br />SURROGATE J <br />o-Terphenyl <br />REPORTING <br />LIMIT <br />UNITS <br />10000 <br />mg/kg <br />50000 <br />mg/kg <br />10000 <br />mg/kg <br />PERCENT RECOVERY <br />RECOVERY LIMITS <br />0.0 SRD (52 - 136) <br />NOTS(S) <br />sRD The wmagate rcwvery was rot aicuiaW use the c=aa was diluted beyond the ability o qu2ndtaw a rocamy. <br />Tbc w"own from n -C16 to n -C40 was quwitita with all peaks from a -C8 to n -C36 and based on moor oU (n -C1910 *4C36). <br />G5C070225 STL Sacramento (916) 373 - 5600 22 of 67 <br />