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MATRIX SPIRE SAMPLE DATA REPORT <br />GC Semivolatiles <br />Client Lot #...: G5C070 25 Work Order #...: G5PG41A.2-MS Matrix.........: SOLID <br />MS Lot -Sample #: G5C070 25-001 G5PG41A3-MSD <br />Date Sampled...: 03/07/05 Date Received..: 03/07/05 <br />Prep Date......: 03/14/05 Analysis Date..: 03/23/05 <br />Prep Batch #...: 5070394 <br />Dilution Factor: 1000 <br />PARAMETER <br />TPH (as Diesel) <br />SURROGATE <br />o-Terphenyl <br />SAMPLE SPIKE MEASRD <br />AMOUNT AMT AMOUNT UNITS <br />ND 10.0 mg/kg <br />Qualifiers: MSA <br />ND 10.0 mg/kg <br />Qualifiers: MSA <br />PERCNT <br />RECVRY RPD METHOD <br />0.0 SW846 8015 MOD <br />0.0 0.0 SW846 8015 MOD <br />PERCENT RECOVERY <br />RECOVERY LIMITS <br />0.0 SRD (52 - 136) <br />0.0 SRD (52 - 136) <br />NOTE(S)- <br />Calculations are performed before rounding to avoid rand -off errors in calculated results. <br />BW pnnt denotes control parameters <br />MSA The recovery and RPD were not calculated because the sample was diluted beyond the ability to quantitate a recovery. <br />SRD The surrogate recovery was not calcula� because the euract was diluted beyond die ability to quantitate a recovery. <br />G5C070225 STL Sacramento (916) 373 - 5600 27 of 67 <br />