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MATRIX SPIRE SAMPLE DATA REPORT <br />TOTAL Metals <br />Client Lot #...: G5C070225 <br />Date Sampled—: 03/07/ 5 Date Received..: 03/07/05 <br />SAMPLE SPIKE MEASRD PERCNT <br />PARAMETER AMOUNT AMT AMOUNT UNITS RECVRY RPD METHOD <br />Vanadium <br />Matrix.......... SOLID <br />57.3 <br />70.4 <br />121 mg/kg <br />90 <br />SW846 <br />6010E <br />57.3 <br />67.0 <br />123 mg/kg <br />98 <br />1.5 SW846 <br />6010B <br />Zinc <br />670 <br />70.4 <br />863 mg/kg <br />SW846 <br />6010B <br />Qualifiers: <br />NC,MSB <br />670 <br />67.0 <br />744 mg/kg <br />SW846 <br />6010B <br />Qualifiers: <br />NC,MSB <br />NOTE (S) : <br />Calculations are performed before roumding b avoid round -off errors in calculated results. <br />Results and reporting Emits have beea adjusted dry weight. <br />NC The recovery aidlor RPD were not calcub ted. <br />M 8 The recovery and RPD were rot calculate I because the sample amount was greater than fora times ft SOM amotuu. <br />N Spiked analyte recovery is outside stated to itrol limits. <br />PREPARATION- WORK <br />ANALYSIS DATE ORDER # <br />03/15-03/18/05 G5P1F1A6 <br />03/15-03/18/05 G5P1F1A9 <br />03/15-03/18/05 G5P1F1CA <br />03/15-03/18/05 G5P1F1CC <br />G5C070225 STL Sacramento (916) 373 - 5600 54 of 67 <br />