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• All samples will be analyzed for Title 22 Metals by EPA Method 6010. Samples with any total <br /> metal concentration greater than or equal to 10 times the respective STLC and below the <br /> TTLC will be further analyzed for soluble metals using EPA Waste Extraction Test (WET) <br /> methods. <br /> • Samples with concentrations at least four times in excess of the standard for a California <br /> Hazardous Waste based on the WET will be analyzed for toxicity characteristic leaching <br /> procedure(TCLP) soluble lead using EPA 1311 to determine if they are also a RCRA waste. <br /> • Soil samples with soluble (WET) metal concentration greater than 5.0 mg/1 will be further <br /> analyzed using deionized water(DI-WET)as extractant following EPA Test Method 7000. <br /> • Ten percent of samples will be analyzed for pH using EPA Test Method 9045 <br /> • Selected soil samples based on field screening will be analyzed for total petroleum <br /> hydrocarbons as gasoline (TPHg); benzene, toluene, ethylbenzene, total xylenes (BTEX); and <br /> methyl tertiary butyl ether(MTBE) using EPA Methods 8015/8021B/8260. <br /> Laboratory QA/QC procedures will be performed for each method of analysis with specificity for each <br /> analyte listed in the test method's QA/QC. QA/QC measures as applicable will include the following: <br /> • One method blank for every ten samples, batch of samples or type of matrix, whichever is <br /> more frequent. <br /> • One sample analyzed in duplicate for every ten samples, batch of samples or type of matrix, <br /> whichever is more frequent. <br /> • One spiked sample for every ten samples, batch of samples or type of matrix, whichever is <br /> more frequent,with the spike made at ten times the detection limit or at the analyte level. <br /> The laboratory will be instructed to homogenize the soil samples tested for metals in accordance with <br /> Contract 06A1141 requirements. <br /> Report Preparation <br /> We will prepare a site investigation report to present our findings and conclusions. The report will <br /> summarize(but not be limited to)the following: <br /> • Project introduction/description <br /> • Investigative methods <br /> • Investigative results and field observations <br /> • Data statistical analysis and discussion <br /> • Conclusions and recommendations <br /> • Tabulated sample analytical data <br /> • Vicinity Map <br /> • Site Plans for each project location that depict boring and sample locations <br /> • Appendices including laboratory reports and COC documentation <br /> SR-99/Monitoring Stations,Task Order No.89 Caltrans Contract 06A1141,EA 10-OK3201 <br /> Project No.S9200-06-89 -4- November 17,2009 <br />