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&PwR laboratories 2905 Railroad Ave. Ceres,CA 95307 (209)581-9280 Fax(209)581-9282 <br /> Lee&Pierce Project Number: EN08640 - ` <br /> 546 Abbott Street,Suite 20 Project Name: Gubary Liquors Work Order No.: <br /> Salinas,CA 93901 <br /> Project Manager: John Lane I806444 <br /> Oxygenates - Method.EPA 82608-Quality Control <br /> Argon Laboratories <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result o/REC Limits RPD Limit Notes <br /> .Batch 180.1291-EPA 5030B <br /> Blank(1801291-BLKI) Prepared&Analyzed:06/16/08 <br /> Surrogate:Fluorobenzene 53.5 ugE 50.0 107 70-130 <br /> t-Butanol ND 5.0 " <br /> Methyl teri-Butyl Ether ND 0.5 " <br /> Di-Isopropyl Ether ND 0.5 " <br /> Ethyl terl-Butyl Ether ND 0.5 <br /> tort-Amyl Methyl Ether ND 0.5 " <br /> 1,2-Dichloroethane ND 0.5 " <br /> 1,2-Dibromoethene(EDB) ND 0,5 " <br /> LCS(1801291-BSI) Prepared&Analyzed:06/16/08 <br /> Methyl tert-Butyl Ether 24.3 uglL 25.0 97 80-120 <br /> LCS Dup(1801291-BSD1) Prepared&Analyzed:06/16/08 <br /> Methyl tert-Bury[Ether 25.3 ug/L 25.0 101 80-120 4 20 <br /> Batch 1801296-EPA 50308 <br /> Blank(1801296-BLKI) Prepared&Analyzed:06/17/08 <br /> Surrogate:Fluoroben.-ene 0.0545 -g'kg 0.0500 109 70-130 <br /> t-Butanol ND 0.050 " <br /> Methyl tert-Butyl Ether ND 0.005 " <br /> Di-Isopropyl Ether ND 0.005 " <br /> Ethyl tert-Bury[Ether ND 0.005 " <br /> tent-Amyl Methyl Ether ND 0.005 " <br /> 12-Dichloroethane ND 0.005 " <br /> 1,2-Dibromoethane(EDB) ND 0.005 " <br /> LCS(1801296-BSI) Prepared&Analyzed:06/17/08 <br /> Methyl tert-Butyl Ether 0.054 mg/kg 0.0500 108 80.120 <br /> LCS Dup(1801296-BSDI) Prepared&Analyzed:06/17/08 <br /> Methyl cert-Butyl Ether 0.054 mglkg 0.0500 108 80-120 0 20 <br /> Approved By <br /> +Argon Laboratories,Inc. California D.O.H.S.Cert.#2359 <br /> Page 5 of 7 <br />