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06L1ill�����11 CQG� CERTIFICATE 4F ANALYSIS <br /> Analytical Laboratory <br /> Tuesday, February 22,2000 <br /> TO. William Little <br /> Advanced GeoEnvironmental, <br /> 4005 N Wilson Way <br /> Stockton, Ca 95205 <br /> Sample Information <br /> Sample ID. AD0210-02 Sample Type- Grab <br /> Sample Description. SBI-10 Project Name: Bogettis Orchard Service <br /> DateJTrme Sampled- 218100 8 30 00 AM Sample Matrix. Soil <br /> ANALYTICAL RESULT QA/QC REPORT <br /> Date LCS Spike MS Spike <br /> Test Parameter Method DLR Unit Result Analyzed Blank Cone. LCS% Cone MS% MSD RSD <br /> i TPH-Gasoline EPA 8015M/DHS 1 mg/Kg 400 11-Feb-00 ND 05 960% 05 920% 940% 05% <br /> TPH-Diesel EPA 8015M1DHS 10 mg/Kg ND 11-Feb-00 ND 100 950% 100 950% 1050% 25% <br /> Methyl t-Butyl Ether(MtBE) EPA8260 5 ug/Kg 2720 11-Feb-00 ND 40 950% 40 1050% 1025% 06% <br /> Dilsopropyl ether(DIPE) EPA8260 5 ug/Kg ND 11-Feb-00 ND 40 900% 40 1050% 1025% 06% <br /> Ethyl-t-butyl ether(ETBE) EPAS260 5 ug/Kg ND 11-Feb-00 ND 40 1050% 40 1025% 1050% 06% <br /> Tort-amyl methyl ether(TAME) EPA8260 5 ug/Kg ND 11-Feb-00 ND 40 900% 40 900% 925% 07% <br /> t-Butanol(TBA) EPA8260 5 ug/Kg ND 11-Feb-00 ND 40 950% 40 975% 875% 27% <br /> Benzene EPA 8260 5 ug/Kg 120 11-Feb-00 ND 40 950% 40 950% 975% 06% <br /> Toluene EPA 8260 5 ug/Kg 50 11-Feb-00 ND 40 1000% 40 975% 950% 06% <br /> Ethyl Benzene EPA 8260 5 ug/Kg 50 11-Feb-00 ND 40 1050% 40 1025% 1050% 0 <br /> Xylene,Total EPA 8260 5 ug/Kg 200 11-Feb-00 ND 80 1000% 80 1125% 1138% 03% <br /> mg/L=milligrams per Luer=ppm DLR-Defection Lmut for the Purpose of Reporting RSD-represent relative percent different(RPD)benveen dupltcates spike of samples <br /> ug/L—micrograms per Luer=ppb Exceptional sample matrices or rnterfereneces may result in or Duplicate of Sample <br /> higher detection limits MS/MSD-measure of the percent recovery of crencres within the matrix <br /> C=Composite G=Grab <br /> LCS-measure of the percent recovery of the Laboratory Control Spike(LCS) <br /> V! TFU ITTED, <br /> Jonathan Hao V. Le,Laboratory Director 1 <br /> EPA-Environmental Protection Agency Method Page 1 of 1 <br /> SM-StandardMethodfor Examrnarront�4t 7E tti{ g8{fJtgt Suite A Stockton, CA 95204 Tel (209) 462-0892 Fax (209) 462-7935 <br />