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CERTIFICATE OF ANALYSIS <br /> Analytical Laboratory <br /> Tuesday, February 21,2000 <br /> ' TO l4rilham Little <br /> Advanced GeoEnv iron mental, <br /> 4005 N Wilson Way <br /> Stockton, Ce 95205 <br /> Sample Information <br /> Sample ID: AD0210-07 Sample Type: Grab <br /> Sample Description: SBI-45 Project Name: Bogettis Orchard Service <br /> Date/Time Sampled: 2/8/00 9 45 00 AM Sample Matrix: Soil <br /> ANALYTICAL RESULT QAIQCREPORT <br /> Date LCS Spike MS Spike <br /> Test Parameter Method DLR Unit Result Analyzed Blank Conc. LCS% Cone. MS% MSD RSD <br /> i TPH-Gasoline EPA 8015MIDHS 1 mg/Kg NO 11-Feb-00 NO 05 960% 05 920% 940% 05% <br /> TPH Diesel EPA 8 mg/Kg 8015M/DHS 10 m IK NO 11-Feb-00 NO 100 950% 100 950% 1050% 25% <br /> Methyl t-Butyl Ether(MtBE) EPA8260 5 ug1Kg NO 11-Feb-00 NO 40 950% 40 1050% 1025% 06% <br /> Dlisopropyl ether(DIPE) EPA8260 5 ug/Kg ND 11-Feb-00 ND 40 900% 40 1050% 102 5% 06% <br /> Ethyl-t-butyl ether(ETRE) EPA8260 5 ug/Kg No 11-Feb-00 NO 40 1050% 40 1025% 1050% 06% <br /> Tert-amyl methyl ether(TAME) EPA8260 5 ug/Kg NO 11-Feb-00 ND 40 900% 40 900% 925% 07% <br /> t-Butanol(TBA) EPA8260 5 ug/Kg NO 11-Feb-00 NO 40 950% 40 975% 875% 27% <br /> Benzene EPA 8260 5 ug/Kg NO 11-Feb-00 NO 40 950% 40 950% 975% 06% <br /> Toluene EPA 8260 5 ug/Kg NO 11-Feb-00 NO 40 1000% 40 975% 950% 06% <br /> Ethyl Benzene EPA 8260 5 ug/Kg NO <br /> 11-Feb-00 ND 40 1050% 40 1025% 1050% 06% <br /> Xylene,Total EPA 8260 5 ug/Kg NO 11-Feb-00 ND 80 1000% 80 1125% 1138% 03% 1 <br /> mg/L=milligrams per Liter=ppm DLR-Detection Limitfor the Purpose of Reporting RSD-represent relative percent different(RPD)between dttplrcates spike ajsanip es <br /> ug/L=micrograms per Liter=ppb Exceptional sample matrices or interferences may result to or Duplicate of Sample <br /> higher detection!units MS/MSD-measure of the percent recovery efficiencies ti+tthm the matror <br /> C=Composite G=Grab <br /> LCS-measure of the percent recovery of the Laboraloiy Control Spike(LCS) <br /> RES TFU ITTED, <br /> Jonathan Hao V Le,Laboratory Director <br /> Page 1 of 1 <br /> EPA-Environmental Protection Agency Method <br /> SM-Standard MethodforExamination534P5aEr T ojiaw444aff y gt Suite A StoCkton, CA 95204 Tel (209) 462-0892 Fax (209) 462-7935 <br />