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o • i <br /> CERTIFICATE OF ANALYSIS <br /> 0!fOAnalytical Laboratory <br /> Tuesday, February 21,2000 <br /> TO. William Little <br /> Advanced GeoEnvlronmental, <br /> 4005 N Wilson Way <br /> Stockton, Ca 95205 <br /> Sample Information <br /> Sample ID AD0210-12 Sample Type: Grab <br /> Sample Description. MW3-10 Project Name: Bogettis Orchard Service <br /> DatelTtme Sampled. 2/9/00 8 35 00 AM Sample Matrix: Soil <br /> ANALYTICAL RESULT QAIQC REPORT <br /> Date LCS Spike MS Spike <br /> Test Parameter Method DLR Unit Result Analyzed Blank Cone LCS% Cone MS% MSD RSD <br /> TPH-Gasoline EPA 8015MJDHS 1 mg/Kg NO 11-Feb-00 NO 05 960% 05 920% 940% 05% <br /> f <br /> TPH-Diesel EPA 8015M/DHS 10 mg/Kg NO 11-Feb-00 ND 100 950% 100 950% 1050% 25% <br /> Methyl t-Butyl Ether(MtBE) EPA8260 5 ug/Kg NO 11-Feb-00 ND 40 950% 40 1050% 1025% 06% <br /> t <br /> Diisopropyl ether(DIPE) EPA8260 5 ug/Kg NO 11-Feb-00 NO 40 900% 40 1050% 1025% 06% <br /> Ethyl-t-butyl ether(ETBE) EPAS260 5 ug/Kg NO 11-Feb-00 ND 40 1050% 40 1025% 1050% 06% <br /> Tort-aroyl methyl ether(TAME) EPA8260 5 ug/Kg NO 11-Feb-00 NO 40 900% 40 900% 925% 07% <br /> ' t-Butanol(TBA) EPA8260 5 ug/Kg ND 11-Feb-00 ND 40 950% 40 975% 875% 27% <br /> Benzene EPA 8260 5 ug/Kg NO 11-Feb-00 ND 40 950% 40 950% 975% 06% <br /> Toluene EPA 8260 5 ug/Kg ND 11-Feb-00 ND 40 1000% 40 975% 950% 06% <br /> Ethyl Benzene EPA$260 5 uglKg ND 11-Feb-00 ND 40 105 0% 40 1025% 1050% 06% <br /> Xylene,Total EPA 8260 5 ug/Kg ND 11-Feb-00 ND 80 1000% 80 1125% 1138% 03% <br /> rng/L=milligrams per Liter=ppm DLR-Detection Limit for the Purpose of Reporting RSD-represent relative percent different(RPD)beh,Ben duplicates rpake of samples <br /> ug/L=micrograms per Liter=ppb Exceptional sample matrices or interfereneces may result in or Duplicate of Sample <br /> higher detection limits MS/MSD-measure of the percent recovery of ciencres it rthm the matrix <br /> C=Composite G=Grab <br /> L(-S-measure of the percent recovery of the Laboratory Control Spike(LC SJ <br /> TFU ITTED, <br /> Jonathan Hao V Le, Laboratory Director <br /> Page I of 1 <br /> EPA-Environmental Protection Agency Method <br /> ' SM-SrandardMethodjor Examination tfr k0ji Vo_giaffd9t Suite A Stockton, CA 95204 Tel (209) 462-0892 Fax (209) 462-7935 <br />