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I <br /> CERTIFICATE OFANAL YSIS <br /> Analytical Laboratory Tuesday,February 22,2000 <br /> TO William Little <br /> Advanced GeoEnvironmental, <br /> 4005 N Wilson Way <br /> E Stockton, Ca 95205 <br /> Sample Information <br /> Sample ID: AD0210-14 Sample Type: Grab <br /> Sample Description: MW4-10 Project Name: Bogettis Orchard Service <br /> DatelTime Sampled. 02/09/2000 It 25 00 AM Sample Matrix. Soil <br /> ANALYTICAL RESULT QAIQCREPORT <br /> Date LCS Spike MS Spike <br /> Test Parameter Method DLR Unit Result Analyzed Blank Cone. LCS% Conc. MS% MSD RSD <br /> TPH-Gasoline EPA 8015WDHS 1 mg/Kg ND 11-Feb-00 ND 05 960% 05 920% 940% 05% <br /> TPH-Diesel EPA 8015M/DHS 10 mg/Kg ND 11-Feb-00 ND 100 950% 100 950% 1050% 25% <br /> Methyl t-Butyl Ether(MtBE) EPA8260 5 ug/Kg 200 11-Feb-00 ND 40 950% 40 1050% 1025% 06% <br /> DilsopropyI ether(101 PE) EPA8260 5 ug/Kg ND 11-Feb-00 ND 40 900% 40 1050% 1025% 06% <br /> Ethyl-t-butyl ether(ETRE) EPA8260 5 ug/Kg ND 11-Feb-00 ND 40 1050% 40 1025% 1050% 06% <br /> Tort-amyl methyl.ether(TAME) EPA8260 5 ug/Kg ND 11-Feb-00 ND 40 900% 40 900% 925% 07% <br /> t-Butanol(TBA) EPA8260 5 ug/Kg ND 11-Feb-00 ND 40 950% 40 975% 875% 27% <br /> Benzene EPA 8260 5 ug/Kg ND 11-Feb-00 ND 40 960% 40 950% 975% 06% <br /> Toluene EPA 8260 5 ug/Kg ND 11-Feb-00 ND 40 1000% 40 975% 950% 06% <br /> Ethyl Benzene EPA 8260 5 ug/Kg ND 11-Feb-00 ND 40 1050% 40 1025% 1050% 06% <br /> l Xylene,Total EPA 8260 5 ug/Kg ND 11-Feb-00 ND 80 1000% 80 1125% 1138% 03% <br /> i mg/L=milligrams per Liter=ppm DLR Detection Limitfor the Purpose of Reporting RSD-represent relative percent different(RPD)between duplicates spike of samptec <br /> I I ug/L=micrograms per Liter=ppb Exceptional sample matrices or interfereneces may result in or Duplicate of Sample <br /> higher detection limits MS/MSD-measure of the percent recovery efftrencies within the matrix <br /> C=Composite G=Grab <br /> LCS measure of the percent recovery of the Laboratory Control Spike(LCS) <br /> i <br /> RESP TFU ITTED, <br /> ; 4 <br /> Jonathan Hao V.Le,Laboratory Director <br /> i � <br /> ' EPA-Environmental Protection Agency Method Page 1 of l <br /> i SMSlandardMethodforExamination!NW&"t O�. e e(,al"W9t Suite A Stockton, CA 95204 Tel (209) 452-0892 Fax (209) 462-7935 <br />