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110 2nd Avenue South,#tD7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL I1VC Telephone 925-798-1620 Fax 925-798-1622 <br /> Ihttp//www mccampbell corn E-mail math@mecampbell corn <br /> Advanced GeoEnvirorimenial Client Project ID Jerry Castro <br /> Date Sampled 09/25/01 <br /> 837 Shaw Road Date Received 10/03/01 <br /> Stockton,CA 95215 Client Contact T1m Cuellar Date Extracted 10/10-10/12/01 <br /> Client P O Date Analyzed 10110-10/12/01 <br /> Seven Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab 1D 80054 180055 80056 80057 <br /> I MW1/ MW2/ MW3/ MW4/ Reporting Limit <br /> Client ID 092501 092501 092501 092501 <br /> Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPS) 11 ND<10 ND<10 ND 50 1 0 <br /> Ethyl tert-Butyl Ether(ETRE) ND<10 ND<10 ND<l0 ND 50 10 <br /> Methyl tert-Butyl Ether(MTBE) 490 ND<10 14 ND 50 1 0 <br /> tert-Amyl Methyl Ether(TAME) ND<10 ND<10 ND<10 ND -10 l 0 <br />' tert-Butanol ND<50 ND<50 ND<50 ND 25 so <br /> Methanol ND<5000 ND<5000 ND<5000 ND 2500 500 <br /> Ethanol ND<500 ND<500 ND<500 ND 250 50 <br />' Surrogate Recoveries(%) <br /> Dibromofluoramethane 104 112 116 111 <br /> Comments j <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP I STLC I SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present (i)liquid sample that contains greater than--5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 P1111— Edward Hamilton, Lab Director <br /> I <br />