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I130 2nd Avenue South #D7 Pacheco,CA 94553-5560 <br /> McCampbell Analytical Inc Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccampbc1l com E-mail rnainPmccampbell corn <br /> 116 <br /> Advanced GeoEnvironmental, Inc Client Project ID Pacific Car Wash Date Sampled 02/25/03 <br />' 837 Shaw Road <br /> Date Received 02/26/03 <br /> Stockton,CA 95215 Client Contact Tun Cuellar Date Extracted 02/26/03-02/28/03 <br />' Client P O Date Analyzed 02/26/03-02/28/03 <br /> Oxygenates and BTEX by GC/MS* <br /> Extraction Method SW5030B Analytical Method SW82608 Work Order 0302345 <br /> Lab 1D 0302345-OOIB 0302345-002B ! 0302345-003B 0302345=004B <br /> Client ID MW1/02-25-03 I MW2/02-25-03 1 MW3/02-25-03 MW4/02-25-03 Reporting Limit for <br />' <br /> Matrix _ _-- W —W ---E----W DF=1 <br /> i <br /> DF 200 100 i 100 T 1 S w <br />' Compound Concentration ug/kg 1AEl <br /> tert-Amyl methyl ether(TAME) ND<100 ND<50 ND<50 ND NA 05 <br />' Benzene 4400 1300 270 ND NA I 05 <br /> t-Butyl alcohol(TBA) ND<1000 ND<500 ND<500 ND NA 50 <br /> 1,2-Dibromoethane(EDB) ND<100 — I ND<50 ND<50 ND NA 05 <br /> 1,2-Dichloroethane(1,2-DCA) Ito ND<50 ND<50 I ND NA i 0 5 <br /> Dilsopropyl ether(DIPE) ND<100 ND<50 ND<50 ND NA 05 <br />' Ethylbenzene 420 3100 1400 ND NA I 05 <br /> Ethyl ter-butyl ether(ETRE) ND<100 ND<50 ND<50 ND NA 05 <br /> Methyl-t-butyl ether(MTBE) 170 ND<50 NIK50 ND NA 0 5 <br /> Toluene 380 3600 100 ND NA 05 <br /> IXylenes — 1500 15,000 2500 ND NA 05 <br /> Surrogate Recoveries(%) <br /> I %SSI 899 863 107 110 <br /> %SS2 111 I 115 111 109 <br /> %SS3 973 933 951 971 <br /> Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in pg/L,soil/sludge/solid samples inµg/kg, wipe samples inµg/wipe, <br /> product/oil/non-aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysts <br /> h)lighter than water immiscible sheen/product is present,1)liquid sample that contains greater than—2 vol %sediment.j)sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 Angela Rydelius, Lab Manager <br /> I <br />