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110 2nd Avenue South,#ED7 Pacheco CA 94553-5560 <br /> EMcCarnpbell Analytical Inc I Telephone 925-798-1620 Fax 925-798 1622 <br /> htcp-1/www mcca bell coin E mail maw maca bell coin <br /> Advanced GeoEnvironmental,Inc Client Project ID Pacific Car Wash Date Sampled 02/25/03 <br /> 837 Shaw Road Date Received 02/26/03 <br /> IClient Contact Tun Cuellar Date Extracted 02/26/03-02128/03 <br /> Stockton,CA 95215 <br /> Client P O Date Analyzed 02126/03-02/28/03 <br /> IOxygenates and BTEX by GCIMS* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0302345 <br /> I Lab ID 0302345-009B 0302345-OIOB y 0302345-011B 0302345-0128 <br /> Client ID MW9/02-25-03 MWIOA/02-25- MW10B/02-25- MW11/02-25-03 <br /> Reporting Limit for <br /> 03— � DF-1 <br /> Mamx ---- W----- - W— I W —�--—W ---- <br /> DF 10 5 ` 5 1 S w <br /> Compound Concentration ug/kg µg�L <br /> tent-Amyl methyl ether(TAME) ND<5 0 ND<2 5 ND<2 5 ND NA 05 <br /> Benzene _ 270 ND<2 5 ND<2 5 ND NA 0 5 <br /> t-Butyl alcohol(TBA) ND<50 ND<25 ND125 ND NA 5 0 <br /> 1,2-Dibromoethane(EDB) ND<5 0 ND<2 5 ND<2 5 ND NA 0 5 <br /> 1,2-Dichloroethane(1,2-DCA) ND<5 0 ND<2 5 ND<2 5 0 71 NA 0 5 <br /> • Dusopropyl ether(DtPE) ND<5 0 ND<2 5 ND<2 5 ND NA 0.5 <br /> Ethylbenzene 170 ND<2 5 ND<2 5 ND NA 0 5 <br /> Ethyl tert-butyl ether(ETBE) ND<5 0 ND<2 5 ND<2 5 ND NA 0 5 <br /> Methyl-t-butyl ether(MTBE) 61 180 130 8 2 NA 05 <br /> Toluene NIK5 0 ND<2 5 ND<2 5 ND NA 05 <br />' Xylenes — --- — 35 ND<2 5 ND<2 5 ND NA 05 <br /> Surrogate Recoveries{%} <br /> I °/aSSI A =103 110 108 114 <br /> %SS2 112 112 112 111 <br />' %SS3 966 100 997 968 <br /> Comments <br /> "water and vapor samples and all 1 CLP&SPLP extracts are reported inµg/L,5oil/sludgelsolid samples in ggilcg, wipe samples toµglwipe, <br /> productloillnon-aqueous liquid samples to mg/L <br />' ND means not detected above the reporting limit,N/A means analyte not applicable to this analysts <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,j)sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 Angela Rydelius,Lab Manager <br />